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Perkin Transactions 1 1972-2002 logo

Year 1993
Main Index

Issue 1


Front cover

pg X001; DOI:
10.1039/P199300FX001
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Contents pages

pg P001; DOI:
10.1039/P199300FP001
PDF
Synthesis of (+)- and (–)-methyl shikimate from benzene
Carl R. Johnson Joseph P. Adams and Mark A. Collins
pg 1; DOI:
10.1039/P19930000001
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A reinvestigation of the intramolecular Buchner reaction of 1-diazo-4-phenylbutan-2-ones leading to 2-tetralones
Alex A. Cordi Jean-Michel Lacoste and Philippe Hennig
pg 3; DOI:
10.1039/P19930000003
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Back cover

pg X003; DOI:
10.1039/P199300BX003
PDF
Formation of cyclic urethanes from amino alcohols and carbon dioxide using phosphorus(III) reagents and halogenoalkanes
Yasuhiko Kubota Masato Kodaka Takenori Tomohiro and Hiroaki (Yohmei) Okuno
pg 5; DOI:
10.1039/P19930000005
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Synthesis and properties of 2,5-dimethylnaphtho[1,8-bc:4,5-bc]dithiophene as a new electron donor
Alec Moradpour
pg 7; DOI:
10.1039/P19930000007
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Back matter

pg P007; DOI:
10.1039/P199300BP007
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Reductive elimination of acetonides, cyclic carbonates, or cyclic sulfites of ,-dihydroxy (E)-,-unsaturated esters: an efficient route to -hydroxy (E)-,-unsaturated esters and -hydroxy esters
Suk-Ku Kang Sung-Gyu Kim Dong-Chul Park Jang-Sup Lee Weon-Jong Yoo and Chwang Siek Pak
pg 9; DOI:
10.1039/P19930000009
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Synthesis of 15N-labelled chiral Boc-amino acids from triflates: enantiomers of leucine and phenylalanine
Fredrik Degerbeck Bengt Fransson Leif Grehn and Ulf Ragnarsson
pg 11; DOI:
10.1039/P19930000011
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Studies on pyrazines. Part 25. Lewis acid-promoted deoxidative thiation of pyrazine N-oxides: new protocol for the synthesis of 3-substituted pyrazinethiols
Nobuhiro Sato Kazunori Kawahara and Noritsugu Morii
pg 15; DOI:
10.1039/P19930000015
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N-benzyloxycarbonylaziridine in the syntheses of 2-aminoethyl armed lariats and selectively N-protected polyazacrown ethers
Mladen ini Sulejman Alihodi and Vinko kari
pg 21; DOI:
10.1039/P19930000021
PDF
Synthesis of fused dihydro-1,2,4-thiadiazolimines from cyano-substituted azides and acyl isothiocyanates
Gerrit L'abbé Ingrid Sannen and Wim Dehaen
pg 27; DOI:
10.1039/P19930000027
PDF
Syntheses of novel 25-hydroxyvitamin D3 haptens having chemical bridges at the C-11 position
Norihiro Kobayashi Akihiko Hisada and Kazutake Shimada
pg 31; DOI:
10.1039/P19930000031
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Reinvestigation of the Pummerer arylation of quinones: a selective approach to 2,2,5-trihydroxybiaryls
Giovanni Sartori Raimondo Maggi Franca Bigi Attilio Arienti and Giuseppe Casnati
pg 39; DOI:
10.1039/P19930000039
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Use of the 1-(2-fluorophenyl)-4-methoxypiperidin-4-yl (Fpmp) protecting group in the solid-phase synthesis of oligo- and poly-ribonucleotides
M. Vaman Rao Colin B. Reese Volker Schehimann and Pak Sang Yu
pg 43; DOI:
10.1039/P19930000043
PDF
C-nucleosides. Part 2. Preparation of 2-[(1R,2S,3R,4R)-2,3-dihydroxy-4-(hydroxymethyl)cyclopentyl]thiazole-4-carboxamide (carbocyclic tiazofurin) and its antipode
Allan P. Dishington David C. Humber and Richard J. Stoodley
pg 57; DOI:
10.1039/P19930000057
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Stereoselective reactions of lithio-vinylsulf oxides with aldehydes
John Fawcett Stuart House Paul R. Jenkins Nicholas J. Lawrence and David R. Russell
pg 67; DOI:
10.1039/P19930000067
PDF
Regio- and face-selective cycloaddition of benzonitrile oxide and C,N-diphenylnitrone to 6,8-dioxabicyclo[3.2.1]oct-3-ene
Alexander J. Blake Ian M. Dawson Angus C. Forsyth Robert O. Gould R. Michael Paton and Desmond Taylor
pg 75; DOI:
10.1039/P19930000075
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Meisenheimer rearrangement of azetopyridoindoles. Part 4. Ring expansion of 2-vinyl-1,2,4,5,10,10b-hexahydroazeto[1,2:1,2]pyrido[3,4-b]indole N-oxides
Takushi Kurihara Yasuhiko Sakamoto Kiyoko Tsukamoto Hirofumi Ohishi Shinya Harusawa and Ryuji Yoneda
pg 81; DOI:
10.1039/P19930000081
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Synthesis and properties of methano-bridged tetradehydro-[20]-, -[24]-, -[26]-, -[28]-, -[30]- and -[32]-annulenediones
Hiroyuki Higuchi Kaori Asano Kaori Nakafuku Yoshie Takai Jro Ojima and Gaku Yamamoto
pg 89; DOI:
10.1039/P19930000089
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Radical-mediated synthesis of the 5,11-methanomorphanthridine ring system: formal total synthesis of montanine-type Amaryllidaceae alkaloids, ()-montanine, ()-coccinine and ()-pancracine
Miyuki Ishizaki Ken-Ichi Kurihara Eiko Tanazawa and Osamu Hoshino
pg 101; DOI:
10.1039/P19930000101
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Photoinduced molecular transformations. Part 137. New general synthesis of 3-substituted 3,4-dihydro-1H-benzo[2]pyran-1-ones (3,4-dihydroisocoumarins)via radical and photochemical fragmentations as the key step
Kazuhiro Kobayashi Atsushi Konishi Yoshikazu Kanno and Hiroshi Suginome
pg 111; DOI:
10.1039/P19930000111
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The application of C8K for organic synthesis: reduction of substituted naphthalenes
Iris S. Weitz and Mordecai Rabinovitz
pg 117; DOI:
10.1039/P19930000117
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Versatile cyclisation reactions using selenoboranes
Tadashi Kataoka Mitsuhiro Yoshimatsu Yoshinori Noda Takashi Sato Hiroshi Shimizu and Mikio Hori
pg 121; DOI:
10.1039/P19930000121
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Unprecedented influence of azides and the effect of bulky groups on zinc-induced reductions of deoxy halogeno sugars
Alois Fürstner Judith Baumgartner and Denis N. Jumbam
pg 131; DOI:
10.1039/P19930000131
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Synthesis of some new isoxazolylacetic acid derivatives
Zsuzsanna Gombos József Nyitrai Gábor Doleschall Pál Kolonits László Párkányi and Alajos Kálmán
pg 139; DOI:
10.1039/P19930000139
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Secondary mould metabolites. Part 41. Structure and biosynthesis of Cercospora beticola toxin (CBT)
Alberto Arnone Gianluca Nasini Lucio Merlini Enzio Ragg and Gemma Assante
pg 145; DOI:
10.1039/P19930000145
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Chiral amplification and the catalytic process in the enantioselective conjugate addition of chiral alkoxydimethylcuprate to (E)-cyclopentadec-2-en-l-one
Kazuhiko Tanaka Junichi Matsui and Hitomi Suzuki
pg 153; DOI:
10.1039/P19930000153
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New synthesis of pyrrolobenzothiazine and pyrrolobenzoxazine ring systems
Charles O. Okafor and Mabel U. Akpuaka
pg 159; DOI:
10.1039/P19930000159
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Corrigendum
Gyula Simig and Manfred Schlosser
pg 163; DOI:
10.1039/P19930000163
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Instructions for authors (1993)

pg viia; DOI:
10.1039/P1993000viia
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IUPAC publications on nomenclature and symbolism

pg xxii; DOI:
10.1039/P1993000xxii
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Conference diary

pg xxix; DOI:
10.1039/P1993000xxix
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Refereeing procedure and policy

pg xxv; DOI:
10.1039/P19930000xxv
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Issue 2


Front cover

pg X005; DOI:
10.1039/P199300FX005
PDF
Back cover

pg X007; DOI:
10.1039/P199300BX007
PDF
Contents pages

pg P013; DOI:
10.1039/P199300FP013
PDF
Back matter

pg P019; DOI:
10.1039/P199300BP019
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Enzyme-catalysed carbon–carbon bond formation: use of transketolase from Escherichia coli
Gordon R. Hobbs Malcolm D. Lilly Nicholas J. Turner John M. Ward Andrew J. Willets and John M. Woodley
pg 165; DOI:
10.1039/P19930000165
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Selective Friedel–Crafts reaction of 26,28-dimethoxycalix[4]arene
Zhi-Tang Huang and Guo-Qiang Wang
pg 167; DOI:
10.1039/P19930000167
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Triterpenoid total synthesis. Part 3. Synthesis of meso- and ()-limatulone, defensive metabolites of the limpet Collisella limatula
Kenji Mori Hirosato Takikawa and Masaru Kido
pg 169; DOI:
10.1039/P19930000169
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Regioselective alkoxydehalogenation of 2,4-dihalogenoquinolines and a reinvestigation of the bromination of 2-methoxyquinoline
Alan G. Osborne and Luke A. D. Miller
pg 181; DOI:
10.1039/P19930000181
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Further radical induced cyclisations of unsaturated sulfones
Iain W. Harvey and Gordon H. Whitham
pg 185; DOI:
10.1039/P19930000185
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Radical induced cyclisations of unsaturated allylic sulfones containing an activating electron withdrawing group
Iain W. Harvey and Gordon H. Whitham
pg 191; DOI:
10.1039/P19930000191
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Synthesis of rigidly linked donor–acceptor systems designed to test the effect of orbital symmetry on the dynamics of long-range intramolecular electron transfer processes
Donald C. Craig Anna M. Oliver and Michael N. Paddon-Row
pg 197; DOI:
10.1039/P19930000197
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Syntheses and spectral characterizations of tricarbonylchromium complexes of calix[4]arenes
Hideshi Iki Taketoshi Kikuchi and Seiji Shinkai
pg 205; DOI:
10.1039/P19930000205
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Studies of phthalazine-5,8-quinone, A ring contraction, and some novel and potentially useful fluorescent phthalimides
John Parrick and Ramanaranjinie Ragunathan
pg 211; DOI:
10.1039/P19930000211
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Synthesis of secotrinervitanes, unique bicyclic diterpenes from termites
Toshifumi Hirukawa Toshiyuki Shudo and Tadahiro Kato
pg 217; DOI:
10.1039/P19930000217
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Photochemical reactions of phenylphosphinic azides having ortho alkyl substituents: diminution of Curtius-like rearrangement; intramolecular nitrene insertion into C–H bonds
Martin J. P. Harger and P. Andrew Shimmin
pg 227; DOI:
10.1039/P19930000227
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Novel formation of 4-methylthiopyrene in a Hofmann elimination reaction directed toward the synthesis of 17,19-dioxa[2.2.3](1,2,3)cyclophanediene
Yee-Hing Lai and Hong-Leng Eu
pg 233; DOI:
10.1039/P19930000233
PDF
Total synthesis of three eudesman-12,8-olides, ()-isoalantolactone, ()-dihydrocallitrisin and ()-septuplinolide; structure revision of septuplinolide
Masahiro Tada Hirokazu Yamada Akira Kanamori and Kazuhiro Chiba
pg 239; DOI:
10.1039/P19930000239
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Structural elucidation of trikoningins KA and KB, peptaibols from Trichoderma koningii
Catherine Auvin-Guette Sylvie Rebuffat Isabelle Vuidepot Marcel Massias and Bernard Bodo
pg 249; DOI:
10.1039/P19930000249
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Nitration of 5-fluoro-2,1,3-benzoselenadiazoles, and the synthesis of 4-fluoro3-nitro-, 4-fluoro-6-nitro-, 5-fluoro-3-nitro-o-phenylenediamines and 3,4-diamino-2-nitrophenols by subsequent deselenation
Wei Tian Spiros Grivas and Kjell Olsson
pg 257; DOI:
10.1039/P19930000257
PDF
Synthesis of squaric acid derivatives by Lewis acid-catalysed reaction of its dichloride, methyl ester chloride, diethylamide chloride, and ethyl diester with unsaturated organosilanes: new method for C–C bond formation on cyclobutenedione
Masatomi Ohno Yoshihiko Yamamoto Yuhichi Shirasaki and Shoji Eguchi
pg 263; DOI:
10.1039/P19930000263
PDF
General methods for synthesizing 2,4-diacylpyrroles and their precursors containing one or two masked acyl groups
Silvano Cadamuro Iacopo Degani Stefano Dughera Rita Fochi Antonella Gatti and Laura Piscopo
pg 273; DOI:
10.1039/P19930000273
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Modifications and extensions of the Pschorr reaction in pyrazole series. Access to the [2]benzopyrano[4,3-c]pyrazole system of pharmaceutical interest
Giuseppe Daidone Salvatore Plescia Benedetta Maggio Vincenzo Sprio Franco Benetollo and Gabriella Bombieri
pg 285; DOI:
10.1039/P19930000285
PDF
A convenient synthesis of some arylated phenylsulfonylacetonitriles and ethyl cyanoacetates using organo-iron complexes
Alaa S. Abd-El-Aziz and Christine R. de Denus
pg 293; DOI:
10.1039/P19930000293
PDF
Sequential pericyclic reactions of unsaturated xanthates. One-pot synthesis of hydrobenzo[c]thiophenes
Kazunobu Harano Masashi Eto Kikuma Ono Keisuke Misaka and Takuzo Hisano
pg 299; DOI:
10.1039/P19930000299
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Conference diary

pg viib; DOI:
10.1039/P1993000viib
PDF

Issue 3


Front cover

pg X009; DOI:
10.1039/P199300FX009
PDF
Back cover

pg X011; DOI:
10.1039/P199300BX011
PDF
Contents pages

pg P021; DOI:
10.1039/P199300FP021
PDF
Back matter

pg P025; DOI:
10.1039/P199300BP025
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Stereochemistry of the formation of lactaldehyde and acetoin produced by the pyruvate decarboxylases of yeast (Saccharomyces sp.) and Zymomonas mobilis: different Boltzmann distributions between bound forms of the electrophile, acetaldehyde, in the two enzymatic reactions
Stephen Bornemann David H. G. Crout Howard Dalton David W. Hutchinson Gregory Dean Nicholas Thomson and Margaret M. Turner
pg 309; DOI:
10.1039/P19930000309
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Conversion of (–)-4-hydroxy-2-oxabicyclo[3.3.0]oct-7-en-3-one into the anti-HIV agent carbovir
Rosemary A. MacKeith Ray McCague Horacio F. Olivo Christopher F. Palmer and Stanley M. Roberts
pg 313; DOI:
10.1039/P19930000313
PDF
Conjugated azoalkenes. Part 14. Synthesis of new 1-amino- and 1,2-diaminopyrrole derivatives by reaction of some conjugated azoalkenes with activated methylene compounds RCH2Ac and RCH2CN (R = aryl, heteroaryl)
Orazio A. Attanasi Zhiyuan Liao Alexander McKillop Stefania Santeusanio and Franco Serra-Zanetti
pg 315; DOI:
10.1039/P19930000315
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(R)-1,3-dimethylcyclopropene—one isomer of the smallest chiral hydrocarbon
Mark S. Baird Helen L. Fitton William Clegg and Andrew McCamley
pg 321; DOI:
10.1039/P19930000321
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Addition of diethyl bromodifluoromethylphosphonate to various alkenes initiated by Co(III)/Zn bimetal redox system
Chang-Ming Hu and Jian Chen
pg 327; DOI:
10.1039/P19930000327
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Synthesis of functionalized organic molecules containing a tetrafluoroethylene fragment by cobaloxime-promoted fluoroalkylation with substituted tetrafluoroethyl bromides
Chang-Ming Hu and Yao-Ling Qiu
pg 331; DOI:
10.1039/P19930000331
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Transformation of carbonyl compounds into gem-difluoro compounds with dibromodifluoromethane/zinc reagent
Chang-Ming Hu Feng-Ling Qing and Cun-Xi Shen
pg 335; DOI:
10.1039/P19930000335
PDF
v-Triazolines. Part 34. Thermal behaviour of 1-(2-aminophenyl)-4,5-dihydro-5-morpholino-1,2,3-triazoles: new synthesis of 2-alkylquinoxalines
Maurizio Battistini Emanuela Erba and Donato Pocar
pg 339; DOI:
10.1039/P19930000339
PDF
Synthesis and highly diastereoselective nucleophilic epoxidation of N-(p-tolylsulfonyl)vinylsulfoximines
Peter L. Bailey William Clegg Richard F. W. Jackson and Otto Meth-Cohn
pg 343; DOI:
10.1039/P19930000343
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Reaction of dicyano epoxides with thiocyanate ion: route to -thiocyanato derivatives or to 2-acetylimino-1,3-oxathioles and X-ray crystal structure of 2-acetylimino-4-(4-tolyl)-1, 3-oxathiole-5-carbonitrile
Alenka Majcen Le Maréchal Albert Robert and Ivan Leban
pg 351; DOI:
10.1039/P19930000351
PDF
Fungal metabolites. Part 5. Rapid structure elucidation of antibiotic peptides, minor components of Trichosporin Bs from Trichoderma polysporum. Application of linked-scan and continuous-flow fast-atom bombardment mass spectrometry
Junko Iida Akira Iida Yoshiko Takahashi Yoshihisa Takaishi Yasuo Nagaoka and Tetsuro Fujita
pg 357; DOI:
10.1039/P19930000357
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Fungal metabolites. Part 6. Nuclear magnetic resonance study of antibiotic peptides, trichosporin Bs, from Trichoderma polysporum
Akira Iida Shinichi Uesato Tetsuro Shingu Masahiro Okuda Yasuo Nagaoka Yoshihiro Kuroda and Tetsuro Fujita
pg 367; DOI:
10.1039/P19930000367
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Fungal metabolites. Part 7. Solution structure of an antibiotic peptide, trichosporin B-V, from Trichoderma polysporum
Akira Iida Shinichi Uesato Tetsuro Shingu Yasuo Nagaoka Yoshihiro Kuroda and Tetsuro Fujita
pg 375; DOI:
10.1039/P19930000375
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Fungal metabolites. Part 8. Primary structures of antibiotic peptides, hypelcin A-I, A-II, A-III, A-IV, A-V, A-VI, A-VII, A-VIII and A-IX from Hypocrea peltata
Kouji Matsuura Akgiil Yesilada Akira Iida Yoshihisa Takaishi Michiko Kanai and Tetsuro Fujita
pg 381; DOI:
10.1039/P19930000381
PDF
Novel one-pot synthesis of 1-iodo-1-trimethylsilyl 1,3-dienes
Yanchang Shen Tielin Wang and Wei Xia
pg 389; DOI:
10.1039/P19930000389
PDF
Conference diary

pg va; DOI:
10.1039/P199300000va
PDF

Issue 4


Front cover

pg X013; DOI:
10.1039/P199300FX013
PDF
Back cover

pg X015; DOI:
10.1039/P199300BX015
PDF
Contents pages

pg P027; DOI:
10.1039/P199300FP027
PDF
Stereoselective C-3 substitution of 1,5-anhydro-2-deoxy-2-formyl-3,4,6-tri-O-methylhex-1-enitols: entry to ribo and xylo series
Cannan Booma and Kalpattu Kuppuswamy Balasubramanian
pg 393; DOI:
10.1039/P19930000393
PDF
Hindered organoboron groups in organic chemistry. Part 22. Some interesting properties of 2,4,6-triisopropylphenylborane (tripylborane, TripBH2), a new useful monoarylborane
Keith Smith Andrew Pelter and Zhao Jin
pg 395; DOI:
10.1039/P19930000395
PDF
Synthesis of 2-alkylcyclohexanones using solvent-free conditions and microwave technology
Jean Pierre Barnier André Loupy Philippe Pigeon Mohamed Ramdani and Patrick Jacquault
pg 397; DOI:
10.1039/P19930000397
PDF
Larger scale preparation of optically-active allylic alcohols
Ethnie Balmer Andrew Germain William P. Jackson and Barry Lygo
pg 399; DOI:
10.1039/P19930000399
PDF
Heptyl 2-cyanopropan-2-yl peroxides from the AIBN-initiated autoxidation of heptane
André Goosen Cedric W. McCleland David H. Morgan Johannes S. O'Connell and Audrey Ramplin
pg 401; DOI:
10.1039/P19930000401
PDF
Studies on the natural -adrenergic receptor antagonist MY336-a: synthesis of a 3-dehydroxymethyl analogue
Teodoro S. Kaufman
pg 403; DOI:
10.1039/P19930000403
PDF
Regioselectivity of radical-induced bond cleavages in epoxides
John A. Murphy and Christopher W. Patterson
pg 405; DOI:
10.1039/P19930000405
PDF
Synthesis of 5-hydroxy-1,7-dioxaspiro[5.5]undec-3-en-2-ones from 2-benzenesulfonyltetrahydropyrans and 5-hydroxybutenolides: X-ray crystal structure determination for (5RS,6SR)-5-acetoxy-4-methoxy3-methyl-1,7-dioxaspiro[5.5]undec-3-en-2-one
Alison M. Baylis Madeleine Helliwell Andrew C. Regan and Eric J. Thomas
pg 411; DOI:
10.1039/P19930000411
PDF
Synthesis of 1,10-seco-5-estr-1 -ynes: potential mechanism-based inhibitors of 3- and 3-hydroxysteroid dehydrogenases
Yuefei Hu and Douglas F. Covey
pg 417; DOI:
10.1039/P19930000417
PDF
Synthesis and spontaneous racemization of benz[a]anthracene 3,4-oxide: photochemical oxygen-walk rearrangements of arene oxides of benz[a]anthracene and triphenylene to yield oxepines
Derek R. Boyd Narain D. Sharma Shiv K. Agarwal Guru S. Gadaginamath Gerard A. O'Kane W. Brian Jennings Haruhiko Yagi and Donald M. Jerina
pg 423; DOI:
10.1039/P19930000423
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Diastereo- and enantio-selectivity in the Pictet–Spengler reaction
Patrick D. Bailey Sean P. Hollinshead Neil R. McLay Keith Morgan Sarah J. Palmer Stephen N. Prince Colin D. Reynolds and Stephen D. Wood
pg 431; DOI:
10.1039/P19930000431
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Use of the kinetically controlled Pictet–Spengler reaction in the asymmetric synthesis of indole alkaloids: formal syntheses of (–)-ajmaline, (–)-koumine, (–)-taberpsychine, (–)-koumidine and (–)-suavoline
Patrick D. Bailey and Neil R. McLay
pg 441; DOI:
10.1039/P19930000441
PDF
An asymmetric route to the demethoxy-fumitremorgins
Patrick D. Bailey Sean P. Hollinshead Neil R. McLay Judith H. Everett Colin D. Reynolds Stephen D. Wood and Federico Giordano
pg 451; DOI:
10.1039/P19930000451
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Asymmetric synthesis of (–)-actinonin and (–)-epi-actinonin
George Bashiardes Graham J. Bodwell and Stephen G. Davies
pg 459; DOI:
10.1039/P19930000459
PDF
Spectroscopic elucidation of glycobismines, first naturally occurring binary acridone alkaloids containing a carbon–carbon linkage
Hiroshi Furukawa Chihiro Ito Tomohisa Ono Tian-Shung Wu and Chang-Sheng Kuoh
pg 471; DOI:
10.1039/P19930000471
PDF
Synthesis of -alkyl--benzyl amino acid derivatives, via the diastereoselective alkylation of (3S,5R)-N,3-dibenzyl-3,4,5,6-tetrahydro-5-phenyl-1,4-oxazin-2-one
Andrew N. Boa Amanda L. Guest Paul R. Jenkins John Fawcett David R. Russell and David Waterson
pg 477; DOI:
10.1039/P19930000477
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Toxic constituents of the asclepiadaceae. Structure elucidation of sarcovimiside A-C, pregnane glycosides of Sarcostemma viminale
Robert Vleggaar Fanie R. van Heerden Lourens A. P. Anderson and Gerdinand L. Erasmus
pg 483; DOI:
10.1039/P19930000483
PDF
Synthesis of (2S,3S)-2-amino-3-methylpent-4-ynoic acid, a precursor amino acid for the preparation of tritium- or deuterium-labelled peptide in the isoleucine residue
Hiroshi Hasegawa Shinichi Arai Yoshihiko Shinohara and Shigeo Baba
pg 489; DOI:
10.1039/P19930000489
PDF
Biosynthetic studies on the decarestrictine family
Marion Mayer and Ralf Thiericke
pg 495; DOI:
10.1039/P19930000495
PDF
Convenient preparations and Michael reactions of 4-fluoroalkylated but-2-en-4-olides
Masato Yoshida Rihoko Imai Yuji Komatsu Yoshihiro Morinaga Nobumasa Kamigata and Masahiko Iyoda
pg 501; DOI:
10.1039/P19930000501
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Some novel reactions of perfluoro-2,3-dialkyloxaziridines
Viacheslav A. Petrov and Darryl D. Desmarteau
pg 505; DOI:
10.1039/P19930000505
PDF
Production of 3- benzoyl-2,1-benzisoxazoles,2-phenyl-4H-3,1-benzoxazin-4-ones, and novel quinolinone derivatives from 2-phenylquinolin-4(1H)-ones and sodium dichloroisocyanurate
Benjamin Staskun and Theodorus van Es
pg 511; DOI:
10.1039/P19930000511
PDF
Structure and conformation of -diphenylphosphinoyl enones: X-ray structure of E-(5SR,6SR)-3,6-dimethyl-5-diphenylphosphinoyl-7-triphenylmethoxyhept-2-en-4-one
Michael J. Doyle David Hall Paul R. Raithby Nicholas Skelton and Stuart Warren
pg 517; DOI:
10.1039/P19930000517
PDF
Synthesis and configurational assignment of methyl 3-nitrooxypropyl 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)pyridine-3,5-dicarboxylate
Toshihisa Ogawa Keita Matsumoto Chihiro Yokoo Katsuo Hatayama and Kunihiro Kitamura
pg 525; DOI:
10.1039/P19930000525
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Hydrodehalogenation of polychlorinated aromatic halides by hypophosphite with Pd/C catalyst under multiphase conditions
Carlos Alberto Marques Maurizio Selva and Pietro Tundo
pg 529; DOI:
10.1039/P19930000529
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Corrigenda
James R. Bull Karl Bischofberger Russell I. Thomson Jan L. M. Dillen Petrus H. van Rooye Thomas Hudlicky Hector Luna Horacio F. Olivo Catherin Anderson Thomas Nugent and John D. Pric
pg 535; DOI:
10.1039/P19930000535
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Conference diary

pg viic; DOI:
10.1039/P1993000viic
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Issue 5


Front cover

pg X017; DOI:
10.1039/P199300FX017
PDF
Back cover

pg X019; DOI:
10.1039/P199300BX019
PDF
Contents pages

pg P033; DOI:
10.1039/P199300FP033
PDF
Back matter

pg P039; DOI:
10.1039/P199300BP039
PDF
Highly functionalised analogues of tetrathiafulvalene: new 9,10-bis(1,3-dithiol-2-ylidene)-9,10-dihydroanthracene donors
Elena Cerrada Martin R. Bryce and Adrian J. Moore
pg 537; DOI:
10.1039/P19930000537
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Concise enantiospecific synthesis of the key intermediate for heteroyohimbine alkaloids: formal synthesis of ajmalicine and 19-epi-ajmalicine
Toshio Honda Naoko Haze Hirohide Ishige Keiko Masuda Koichi Naito and Yukio Suzuki
pg 539; DOI:
10.1039/P19930000539
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Novel gibberellin ring a epoxy alcohols: synthesis and X-ray molecular structure
Martin Penny Christine L. Willis Andrei S. Batsanov and Judith A. K. Howard
pg 541; DOI:
10.1039/P19930000541
PDF
Autorecycling system for reduction of carbonyl compounds to alcohols by 1,5-dihydro-5-deazaflavins
Kazunori Kuroda Tomohisa Nagamatsu Reiko Yanada and Fumio Yoned
pg 547; DOI:
10.1039/P19930000547
PDF
Phosphorus-based reagents in peptide synthesis: synthesis of methionine-enkephalin and the solution conformation of its N-diphenylphosphinoyl derivative
D. David Smith Kenneth G. Boyd David Hopton Robert L. Baxter and Robert Ramage
pg 551; DOI:
10.1039/P19930000551
PDF
Enzymatic preparation of enantiomerically pure alkan-2- and -3-ols by lipase-catalysed hydrolysis with Pseudomonas cepacia in the presence of organic media
Yoshinobu Naoshima Makoto Kamezawa Hojun Tachibana Yoshihito Munakata Tomoki Fujita Kohei Kihara and Takao Raku
pg 557; DOI:
10.1039/P19930000557
PDF
Highly diastereoselective aldol reactions of cobalt-complexed and uncomplexed propynals with O-silyl ketene O,S-ketals: highly stereoselective divergent formal syntheses of the -lactam antibiotics ()-PS-5 and ()-epi-PS-5
Chisato Mukai Osamu Kataoka and Miyoji Hanaoka
pg 563; DOI:
10.1039/P19930000563
PDF
Peptides from australian frogs. Structures of the caeridins from Litoria caerulea
Russell J. Waugh David J. M. Stone John H. Bowie John C. Wallace and Michael J. Tyler
pg 573; DOI:
10.1039/P19930000573
PDF
Diastereoselective synthesis of cyclopropanes with multiple sulfur substitution. X-Ray molecular structures of phenylsulfonyl-substituted cyclopropanes
Peter L. Bailey Cheryl T. Hewkin William Clegg and Richard F. W. Jackson
pg 577; DOI:
10.1039/P19930000577
PDF
Novel rearrangement of 2--isopropyl-8-oxabicyclo[3.2.1]oct-6-ene producing the monoterpene 3-hydroxyphellandral
Luiz Claudio de Almeida Barbosa Antonio J. Demuner John Mann and Dorila P. Veloso
pg 585; DOI:
10.1039/P19930000585
PDF
Enzymatic regioselective alkoxycarbonylation of hexoses and pentoses with carbonate oxime esters
Rosalino Pulido and Vicente Gotor
pg 589; DOI:
10.1039/P19930000589
PDF
A new approach to piperidine alkaloids: an enantioselective total synthesis of (2S,6R)- and (2R,6S)-dihydropinidine
Zhi-Hui Lu and Wei-Shen Zhou
pg 593; DOI:
10.1039/P19930000593
PDF
Approaches to chemically modified enzymes as synthetic catalysts
David J. Aitken Renate Alijah Samuel O. Onyiriuka Colin J. Suckling Hamish C. S. Wood and Limin Zhu
pg 597; DOI:
10.1039/P19930000597
PDF
Manganese-(II) and (III)-mediated free-radical cyclisation of alkenes, -keto esters and molecular oxygen
Takashi Yamada Yoko Iwahara Hiroshi Nishino and Kazu Kurosawa
pg 609; DOI:
10.1039/P19930000609
PDF
Absolute configuration of tautomycin, a protein phosphatase inhibitor from a streptomycete
Makoto Ubukata Xing-Chun Cheng Minoru Isobe and Kiyoshi Isono
pg 617; DOI:
10.1039/P19930000617
PDF
Silylation of azole N-oxides
Mikael Begtrup and Per Vedsø
pg 625; DOI:
10.1039/P19930000625
PDF
N-alkenyl nitrone dipolar cycloaddition routes to piperidines and indolizidines. Part 5. Preparation of a gephyrotoxin precursor
Andrew B. Holmes Andrew B. Hughes and Adrian L. Smith
pg 633; DOI:
10.1039/P19930000633
PDF
Conference diary

pg viid; DOI:
10.1039/P1993000viid
PDF

Issue 6


Front cover

pg X021; DOI:
10.1039/P199300FX021
PDF
Back cover

pg X023; DOI:
10.1039/P199300BX023
PDF
Contents pages

pg P041; DOI:
10.1039/P199300FP041
PDF
Back matter

pg P045; DOI:
10.1039/P199300BP045
PDF
Photoinduced electron-transfer reaction of difluorodiiodomethane with azaaromatic compounds and enamines
Qing-Yun Chen and Zhan-Ting Li
pg 645; DOI:
10.1039/P19930000645
PDF
Indirect electroreductive addition of alkyl radicals to activated olefins using a nickel(II) complex as an electron-transfer catalyst
Shigeko Ozaki Hidenori Matsushita and Hidenobu Ohmori
pg 649; DOI:
10.1039/P19930000649
PDF
Synthesis of 4,8-bis(4-hydroxy-3-methoxyphenyl )-3,7-dioxabicyclo[3.3.0]octan-2-ones and determination of their relative configuration via long-range proton couplings
Stéphane Quideau and John Ralph
pg 653; DOI:
10.1039/P19930000653
PDF
Photochemistry of N-heterocycles. Part 3. Synthesis and photochemistry of some new dihydro-1,2,4-triazines and their quaternary salts
József Nagy Rudolf Rapp Mária Alexovics Dietrich Döpp József Nyitrai Uwe Záhorszky and Herbert Röttele
pg 661; DOI:
10.1039/P19930000661
PDF
Synthesis of ()-thaps-7(15)-ene and ()-thaps-6-enes
Adusumilli Srikrishna and Kathiresan Krishnan
pg 667; DOI:
10.1039/P19930000667
PDF
Studies on Wallach's imidazole synthesis
Tiziana Benincori Elisabetta Brenna and Franco Sannicolo
pg 675; DOI:
10.1039/P19930000675
PDF
Migratory tendencies for 1,5-sigmatropic shifts in the 1,3-dimethylindene system
David W. Jones and Robert J. Marmon
pg 681; DOI:
10.1039/P19930000681
PDF
Synthesis and trehalase-inhibitory activity of an imino-linked dicarba-,-trehalose and analogues thereof
Seiichiro Ogawa Koji Sato and Yasunobu Miyamoto
pg 691; DOI:
10.1039/P19930000691
PDF
Synthesis and catalytic properties of 5-deazaflavo-6,9-quinones
Tetsutaro Kimachi Yoshinori Tamura Kiyoshi Bessho and Fumio Yoneda
pg 697; DOI:
10.1039/P19930000697
PDF
Asymmetric synthesis of optically active phthalides via ortho-lithiation and cyclization of chiral N-monosubstituted benzamides
Syuichi Matsui Akinori Uejima Yoshinori Suzukia and Kazuhiko Tanaka
pg 701; DOI:
10.1039/P19930000701
PDF
Synthesis and reactions of [1,2,4]triazolo[4,3-a]pyridinium-3-aminides and [1,2,4]triazolo[4,3-a]pyrimidinium-3-aminides: evaluation of the scope and mechanism of a new type of heterocyclic rearrangement
Brian C. Bishop Hugh Marley Kevin J. McCullough Peter N. Preston and Stanley H. B. Wright
pg 705; DOI:
10.1039/P19930000705
PDF
Sigmatropic rearrangement of 3-(aryloxymethyl)coumarins: a simple synthesis of hydroxylated 3-benzylcoumarins
Krishna C. Majumdar Subrata Saha Rathindra N. De and Santosh K. Ghosh
pg 715; DOI:
10.1039/P19930000715
PDF
Biscyclophanes. Part 2: Regioselectivity in the acid-catalysed cycloalkylation of benzylbenzylic alcohol (BBA)
Woo Young Lee Wonbo Sim Hyo-Joong Kim and Sung-Hwa Yoon
pg 719; DOI:
10.1039/P19930000719
PDF
Heterocyclic transformations. Part 5: Studies in reactions of 6-methyl -l,3-oxazine-2,4(3H)-dione with arylamines—a facile synthesis of 1-aryl-6-methyluracils
Harjit Singh Palwinder Singh Pawan Aggarwal and Subodh Kumar
pg 731; DOI:
10.1039/P19930000731
PDF
Preferential oxygenation of 4-cycloalkylideneoxazol-5(4H)-ones: synthesis of N-acylcycloalk-1-enecarboxamides
Nagabundi Lalitha Uday Triamakraj Bhalerao and Divi Sarangapani Iyengar
pg 737; DOI:
10.1039/P19930000737
PDF
Cadmium iodide as a new catalyst for knoevenagel condensations
Dipak Prajapati and Jagir S. Sandhu
pg 739; DOI:
10.1039/P19930000739
PDF
Conference diary

pg vb; DOI:
10.1039/P199300000vb
PDF

Issue 7


Front cover

pg X025; DOI:
10.1039/P199300FX025
PDF
Back cover

pg X027; DOI:
10.1039/P199300BX027
PDF
Contents pages

pg P049; DOI:
10.1039/P199300FP049
PDF
Back matter

pg P055; DOI:
10.1039/P199300BP055
PDF
General synthesis of inositols by hydrolysis of conduritol epoxides obtained biocatalytically from halogenobenzenes: (+)-D-chiro-inositol, allo-inositol, muco-inositol and neo-inositol
Martin Mandel and Tomas Hudlicky
pg 741; DOI:
10.1039/P19930000741
PDF
Oxidative rearrangements of alkyl substituted isoquinoline enamides to 1-hydroxymethyldihydroisoquinoline derivatives
George R. Lenz Ralph A. Lessor Patrice W. Rafalko and Zenyk Kosarych
pg 745; DOI:
10.1039/P19930000745
PDF
Facile preparation of cyclic oligoribonucleotides
L. De Napoli A. Galeone L. Mayol A. Messere G. Piccialli and C. Santacroce
pg 747; DOI:
10.1039/P19930000747
PDF
Two unexpected but understandable reactions with lithium diisopropylamide (LDA)
Sarah C. Archibald and Ian Fleming
pg 751; DOI:
10.1039/P19930000751
PDF
The reaction of aldehydes and ammonium acetate with some acetonyl and phenacyl derivatives: a correction
Conor N. O'Callaghan and T. Brian H. McMurry
pg 755; DOI:
10.1039/P19930000755
PDF
Total synthesis of (–)-C34-botryococcene, the principal triterpenoid hydrocarbon of the freshwater alga Botryococcus braunii
James D. White G. Nagabushana Reddy and Gary O. Spessard
pg 759; DOI:
10.1039/P19930000759
PDF
Cyclopenta-1,2,3-dithiazoles and related compounds
M. John Plater Charles W. Rees David G. Roe and Tomás Torroba
pg 769; DOI:
10.1039/P19930000769
PDF
Synthesis of new liquid crystalline compounds based on 1,4-diarylbuta-1,3-dienes
Roger Brettle David A. Dunmur Nigel J. Hindley and Charles M. Marson
pg 775; DOI:
10.1039/P19930000775
PDF
Cleavage of steroidal -hydroxy acetals with methylmagnesium iodide
George A. Morrison and William J. W. Watson
pg 783; DOI:
10.1039/P19930000783
PDF
2,2-Difluoro enol silyl ethers: convenient preparation and application to the synthesis of a novel fluorinated brassinosteroid
Fuqiang Jin Yuanyao Xu and Weiyuan Huang
pg 795; DOI:
10.1039/P19930000795
PDF
General synthesis of methyl- and dimethyl -cyclobutanes from simple 1,3-diols by phase transfer catalysis
Béla Török and Árpád Molnár
pg 801; DOI:
10.1039/P19930000801
PDF
Applications of biotransformations in organic synthesis: preparation of enantiomerically pure esters of cis- and trans-epoxysuccinic acid
David H. G. Crout Véronique S. B. Gaudet and Keith O. Hallinan
pg 805; DOI:
10.1039/P19930000805
PDF
Selenium transfer reagent: one-step alkoxyselenation of cyclohexene with bis(2-bromoethyl)selenium dibromide
Yoshinori Takanohashi Narumi Tabata Tomoaki Tanase and Sadatoshi Akabori
pg 813; DOI:
10.1039/P19930000813
PDF
Approaches to pseudopeptidic ergopeptines. Synthesis and molecular structure of an -aza-phenylalanine-containing oxa-cyclol
Francesco Pinnen Grazia Luisi Gino Lucente Enrico Gavuzzo and Silvio Cerrini
pg 819; DOI:
10.1039/P19930000819
PDF
Photoinduced molecular transformations. Part 138. A new route to dibenzo[a,d]cycloalkanes and their naphtho analogues via the ring expansion of benzocyclobutenols involving a selective -scission of cyclobutenoxyl radicals generated by photolysis of their hypoiodites
Kazuhiro Kobayashi Atsushi Konishi Masahito Itoh and Hiroshi Suginome
pg 825; DOI:
10.1039/P19930000825
PDF
Preparation of enantiomerically pure phosphine oxides by nucleophilic displacement chemistry using oxazaphospholidines
Joseph V. Carey Michael D. Barker John M. Brown and Michael J. H. Russell
pg 831; DOI:
10.1039/P19930000831
PDF
Disaccharides to inositol saccharides: synthesis of -D-galactopyranosyl-D-myo-inositol derivatives from a methyl 4-O-(-D-galactopyranosyl)--D-glucopyranoside derivative
Hari Babu Mereyala and Sreenivasulu Guntha
pg 841; DOI:
10.1039/P19930000841
PDF
Synthesis and biological evaluation of 4-quinolone ribosides
Angeles de la Cruz José Elguero Pilar Goya Ana Martineza and Erik De Clercq
pg 845; DOI:
10.1039/P19930000845
PDF
Reactions of trico-ordinate phosphorus compounds with phosphorus pseudohalogens. Part 2. Pentaco-ordinate intermediates in the reaction of o-phenylene neopentyl phosphite with diethoxyoxophosphoranesulfenyl chloride
Ewa Krawczyk Aleksandra Skowroska Jan Michalski and Jerzy Mikoajczak
pg 851; DOI:
10.1039/P19930000851
PDF
Simple synthesis of dimethyl 4-methyl-6-perfluoroalkylisophthalates and dimethyl 5-perfluoroalkylbiphenyl-2,4-dicarboxylates via acyclic precursors
Ding Weiyu Cao Weiguo Xu Zhenrong Yao Yuan Shi Zhijian and Han Zhiheng
pg 855; DOI:
10.1039/P19930000855
PDF
Facile control of regioselectivity in the reaction of tin enolates with -halogeno carbonyls by additives
Makoto Yasuda Tatsuhiro Oh-Hata Ikuya Shibata Akio Baba and Haruo Matsuda
pg 859; DOI:
10.1039/P19930000859
PDF
Direct aromatic amination by azides: reactions of hydrazoic acid and butyl azides with aromatic compounds in the presence of both trifluoromethanesulfonic acid and trifluoroacetic acid
Hiroshi Takeuchi Taki Adachi Hideaki Nishiguchi Katsutaka Itou and Kikuhiko Koyama
pg 867; DOI:
10.1039/P19930000867
PDF
The preparation of the (6R)- and (6S)-diastereoisomers of 5-formyltetrahydrofolate (leucovorin)
Jonathan Owens Lilias Rees Colin J. Suckling and Hamish C. S. Wood
pg 871; DOI:
10.1039/P19930000871
PDF
Corrigendum
Philip C. Bulman Page and David C. Jennens
pg 877; DOI:
10.1039/P19930000877
PDF
Conference diary

pg viie; DOI:
10.1039/P1993000viie
PDF

Issue 8


Front cover

pg X029; DOI:
10.1039/P199300FX029
PDF
Back cover

pg X031; DOI:
10.1039/P199300BX031
PDF
Contents pages

pg P059; DOI:
10.1039/P199300FP059
PDF
Back matter

pg P065; DOI:
10.1039/P199300BP065
PDF
Synthesis of norsegoline
Stephen H. Dunn and Alexander McKillop
pg 879; DOI:
10.1039/P19930000879
PDF
Biooxidations of some N-arylpiperidines and related compounds using Beauveria sulfurescens
Nicholas Floyd Francois Munyeman Stanley M. Roberts and Andrew J. Willetts
pg 881; DOI:
10.1039/P19930000881
PDF
Substituted 1-(21-aminovinyl)pyrroles and pyrrolo[1,2-a]pyrazines from the reaction of a pyrazolium methanide 1,3-dipole with dialkyl acetylenedicarboxylates: a 1,2-carbon to nitrogen rearrangement in the pyrazole system
Richard N. Butler Helena A. Gavin D. Cunningham and Patrick McArdle
pg 883; DOI:
10.1039/P19930000883
PDF
Asymmetric synthesis. Part 19. Asymmetric autocatalysis of (R)-1-phenylpropan-1-ol mediated by a catalytic amount of amine in the addition of diethylzinc to benzaldehyde
Li ShengJian Jiang Yaozhong Mi Aiqiao and Yang Guishu
pg 885; DOI:
10.1039/P19930000885
PDF
Tailor-making of desired assemblies from well-designed monomers: use of calix[4]arene conformers as building blocks
Susumu Arimori Takeshi Nagasaki and Seiji Shinkai
pg 887; DOI:
10.1039/P19930000887
PDF
Homolytic reactions of ligated boranes. Part 17. Amine–boranes as polarity reversal catalysts for radical chain reactions of esters with vinylic epoxides and with allylic tert-butyl peroxides
Hai-Shan Dang and Brian P. Roberts
pg 891; DOI:
10.1039/P19930000891
PDF
Enzymic polymerisation of an unactivated diol/diacid system
Falmai Binns Stanley M. Roberts Alan Taylor and Charles F. Williams
pg 899; DOI:
10.1039/P19930000899
PDF
Hetero-analogues of Hckel degenerate systems and related compounds: preparation of thienyl-substituted fulvalene and electron-donating tetrathiafulvalene vinylogues and conductive complexes
Akira Ohta Tomoshige Kobayashi and Hiroshi Kato
pg 905; DOI:
10.1039/P19930000905
PDF
Two-step approach towards the accelerated synthesis of dendritic macromolecules
Ralph Spindler and Jean M. J. Fréchet
pg 913; DOI:
10.1039/P19930000913
PDF
Synthesis of cyclo-bis[7, 12-diacetoxy-3-dicyanomethyl-3-(4-methylenephenyl)cholanamide]; a cholaphane with reduced flexibility and externally-directed functionality
Anthony P. Davis and Michael G. Orchard
pg 919; DOI:
10.1039/P19930000919
PDF
Small-scale solid-phase O-glycopeptide synthesis of linear and cyclized hexapeptides from blood-clotting factor IX containing O-(-D-Xyl-13--D-Xyl-13--D-Glc)-L-ser
Kerry B. Reimer Morten Meldal Shoichi Kusumoto Koichi Fukaseb and Klaus Bocka
pg 925; DOI:
10.1039/P19930000925
PDF
Synthesis of met- and leu-enkephalin analogues containing chiral N,N-ethylene-bridged phenylalanyl-methionine and -leucine
Hiroshi Takenaka Hiroyuki Miyake Yoshitane Kojima Masahide Yasuda Munekazu Gemba and Tetsushi Yamashita
pg 933; DOI:
10.1039/P19930000933
PDF
Oxazolo[3,2-a]indoles, pyrrolo- and azepino-[1,2-a]indoles from 3H-indole 1-oxides and acetylenecarboxylic esters by skeletal rearrangements
Roy M. Letcher Della W. M. Sin and Kung-Kai Cheung
pg 939; DOI:
10.1039/P19930000939
PDF
Generation and solution-phase behaviour of some 2-halogeno-1,3-ring-fused cyclopropenes
Martin G. Banwell Madelaine Corbett Jacqueline Gulbis Maureen F. Mackay and Monica E. Reum
pg 945; DOI:
10.1039/P19930000945
PDF
Synthesis of imidazoles by the oxidative transformation of 5-aminopyrimidinones
Izumi Matsuura Taisei Ueda Nobutoshi Murkami Shin-ichi Nagai Akito Nagatsu and Jinsaku Sakakibara
pg 965; DOI:
10.1039/P19930000965
PDF
-Pyrones. Part 4. Synthesis of 3-benzoylamino-6-(indol-2-yl)pyran-2-ones and their rearrangement to substituted azepino[1,2-a]indole-6-ones: unusual neighbouring group participation
M. Luisa Gelmi Donato Pocar and Fulvio Vago
pg 969; DOI:
10.1039/P19930000969
PDF
Synthesis of methano-bridged tetradehydrodiaza[22]annulene and related compounds
Hiroyuki Higuchi Hiroyuki Yamamoto Jro Ojima and Gaku Yamamoto
pg 975; DOI:
10.1039/P19930000975
PDF
Synthesis of methano-bridged tetradehydro[36]annulene
Hiroyuki Higuchi Hiroyuki Yamamoto Jro Ojima Masahiko Iyoda Masato Yoshidab and Gaku Yamamoto
pg 983; DOI:
10.1039/P19930000983
PDF
Retinoids and related compounds. Part 14. A novel synthesis of conjugated 4-alkylidenebutenolides and their spectral characterization
Masayoshi Ito Yuko Katsuta Yumiko Yamano and Kiyoshi Tsukida
pg 987; DOI:
10.1039/P19930000987
PDF
Synthetic studies on the C/D ring segment of limonoids
Marc Renoud-Grappin Corinne Vanucci and Gérard Lhommet
pg 995; DOI:
10.1039/P19930000995
PDF
Conference diary

pg viif; DOI:
10.1039/P1993000viif
PDF

Issue 9


Front cover

pg X033; DOI:
10.1039/P199300FX033
PDF
Back cover

pg X035; DOI:
10.1039/P199300BX035
PDF
Contents pages

pg P071; DOI:
10.1039/P199300FP071
PDF
Back matter

pg P077; DOI:
10.1039/P199300BP077
PDF
Microwave-assisted deacetylation on alumina: a simple deprotection method
Rajender S. Varma Manju Varma and Arnab K. Chatterjee
pg 999; DOI:
10.1039/P19930000999
PDF
Enzymatic synthesis of -galactosyloxime derivatives using -galactosidase
Marcos Pozo and Vicente Gotor
pg 1001; DOI:
10.1039/P19930001001
PDF
Displacement reactions on 2,3,4,6-tetra-O-benzyl-1,5-di-O-sulfonyl-D-glucitols. Synthesis of (3R,4S)-3,4-dibenzyloxy-2-(2-benzyloxyethylidene)tetrahydrofuran
Paul A. Fowler Alan H. Haines Richard J. K. Taylor Ewan J. T. Chrystal and Michael B. Gravestock
pg 1003; DOI:
10.1039/P19930001003
PDF
Synthesis of anabasine-6-carboxylic acid from aldosine, the aldol crosslinking amino acid of elastin
Fumihiko Nakamura and Kyozo Suyama
pg 1007; DOI:
10.1039/P19930001007
PDF
Chemistry of silyl thioketones. Part 7. Synthesis, cycloaddition and oxidation of cycloalkyl silyl thioketones and desilylation of the reaction products
Bianca F. Bonini Filippo Busi Roland C. de Laet Germana Mazzanti Jan-Willem J. F. Thuring Paolo Zanies and Binne Zwanenburg
pg 1011; DOI:
10.1039/P19930001011
PDF
Structure and synthesis of arnottin I: a 6H-benzo[d]naphtho[1, 2-b]pyran-6-one derivative from a plant source
Hisashi Ishii Tsutomu Ishikawa Masayuki Murota Yoshiyuki Aoki and Takashi Harayama
pg 1019; DOI:
10.1039/P19930001019
PDF
Organometallic fulgides. Part 1. Synthesis and photochemistry of ferrocenyl fulgides [ferrocenylethylidene(isopropylidene)succinic anhydrides]
Richard W. McCabe David E. Parry and Stephen P. Saberia
pg 1023; DOI:
10.1039/P19930001023
PDF
A novel and stereodefined synthesis of (E)--ethoxycarbonylvinylsilanes: regio- and stereo-controlled hydroethoxycarbonylation of silylacetylenes by palladium(II) catalysis
Ryo Takeuchi and Masaharu Sugiura
pg 1031; DOI:
10.1039/P19930001031
PDF
A study of the reactions of N-methylnitrilium trifluoromethanesulfonate salts with benzylidenetriphenylphosphorane
Brian Beagley Pogu Bitrus Brian L. Booth and Robin G. Pritchard
pg 1039; DOI:
10.1039/P19930001039
PDF
Reaction of N-substituted acetohydrazides with 2-substituted cinnamonitriles. Competitive cyclizations to pyrazolo[3,4-b]pyridinones and [1,2,4]triazolo[1,5-a]pyridinones
Ali Hadi Nazario Martín Carlos Seoane and José L. Soto
pg 1045; DOI:
10.1039/P19930001045
PDF
Synthesis of carboranyl phenylalanine for potential use in neutron capture therapy of melanoma
Jognandan K. Prashar and Douglas E. Moore
pg 1051; DOI:
10.1039/P19930001051
PDF
Heterocycles by cycloaddition. Part 10. Cycloaddition–extrusion–ring expansion of mesoionic compounds with benzocyclobutene. Approaches to seven- and eight-membered fully conjugated systems
Hiroshi Kato Tomoshige Kobayashi Kayo Horie Kotomi Oguri and Masayuki Moriwaki
pg 1055; DOI:
10.1039/P19930001055
PDF
Synthesis of 2,3,6,7-tetrahydro- and 2,3,4,5,6,7-hexahydro-1H-1,4-diazepines via a tandem Michael-type addition–intramolecular aza-Wittig sequence
Aziza Benalil Andrea Guerin Bertrand Carboni and Michel Vaultier
pg 1061; DOI:
10.1039/P19930001061
PDF
Structure and stereochemistry of cis-dihydro diol and phenol metabolites of bicyclic azaarenes from Pseudomonas putida UV4
Derek R. Boyd Narain D. Sharma Michael R. J. Dorrity Mark V. Hand R. Austin S. McMordie John F. Malone H. Patricia Porter Howard Dalton Jagdeep Chima and Gary N. Sheldrake
pg 1065; DOI:
10.1039/P19930001065
PDF
Preparation and enantiomer recognition behaviour of crown ethers containing cis-1-phenylcyclohexane-1,2-diol and trans-1,2-diphenylcyclohexane-1,2-diol as a chiral subunit
Koichiro Naemura Hajime Miyabe Yasuhiro Shingai and Yoshito Tobe
pg 1073; DOI:
10.1039/P19930001073
PDF
Selective lithiation of bis(azol-1-yl)methanes
Enrique Diez-Barra Antonio de la Hoz Ana Sánchez-Migallón and Juan Tejeda
pg 1079; DOI:
10.1039/P19930001079
PDF
Further investigation on the reaction of heterocyclic ketene aminals with ethyl propiolate: ene-type reaction of enamines and an unusual substituent effect
Zhi-Tang Huang and Mei-Xiang Wang
pg 1085; DOI:
10.1039/P19930001085
PDF
Conference diary

pg viig; DOI:
10.1039/P1993000viig
PDF

Issue 10


Front cover

pg X037; DOI:
10.1039/P199300FX037
PDF
Back cover

pg X039; DOI:
10.1039/P199300BX039
PDF
Contents pages

pg P079; DOI:
10.1039/P199300FP079
PDF
Application of an intramolecular Michaelis–Arbusov reaction to the synthesis of nucleoside 3-S,5-O-cyclic phosphorothiolate triesters
Xiang Li and Richard Cosstick
pg 1091; DOI:
10.1039/P19930001091
PDF
Enzymatic resolution of oxalate esters of a tertiary alcohol using porcine pancreatic lipase
Ian Brackenridge Raymond McCague Stanley M. Roberts and Nicholas J. Turner
pg 1093; DOI:
10.1039/P19930001093
PDF
Total synthesis of (+)-kifunensine, a potent glycosidase inhibitor
Jacques Rouden and Tomas Hudlicky
pg 1095; DOI:
10.1039/P19930001095
PDF
Investigation of the regioselectivity of some esterifications involving methyl 4,6-O-benzylidene D-pyranosides and Pseudomonas fluorescens lipase
Gilles Iacazio and Stanley M. Roberts
pg 1099; DOI:
10.1039/P19930001099
PDF
Studies on quinones. Part 27. Diels–Alder reaction of 8,8-dimethylnaphthalene-1,4,5(8H)-trione
Jaime A. Valderrama Ramiro Araya-Maturana and Fernando Zuloaga
pg 1103; DOI:
10.1039/P19930001103
PDF
Preparation of a novel potent inhibitor of methylthioadenosine nucleosidase
David Hendry Edward J. Hutchinson Stanley M. Roberts Steven M. Dunn and John A. Bryant
pg 1109; DOI:
10.1039/P19930001109
PDF
Direct conversion of alcohols into thiols
Takehiko Nishio
pg 1113; DOI:
10.1039/P19930001113
PDF
Reactivity of 1,1-disubstituted indazol-3-ylio oxides: synthesis of some substituted indazolols and indazolinones
Vicente J. Arán Juan L. Asensio José R. Ruiz and Manfred Stud
pg 1119; DOI:
10.1039/P19930001119
PDF
Formation of chiral -lactams by photocyclisation of achiral N,N-diisopropylarylglyoxylamides in their chiral crystalline form
Fumio Toda and Hisakazu Miyamoto
pg 1129; DOI:
10.1039/P19930001129
PDF
Telluroxide elimination by oxidation of alkyl aryl tellurides: remarkable effect of added triethylamine
Yoshiaki Nishibayashi Naoki Komatsu Kouichi Ohe and Sakae Uemura
pg 1133; DOI:
10.1039/P19930001133
PDF
Aziridines. Part 60. Electron transfer from radical anions to N-alkanoylaziridines. Exocyclic cleavage of an aziridino ketyl
Pen-Yuan Lin Jürgen Werry Gunther Bentz and Helmut Stamm
pg 1139; DOI:
10.1039/P19930001139
PDF
Preparation of all-trans-(1,4-phenylenehexa-1,3,5-trienylene) oligomers
Yoriko Sonoda and Yukimichi Nakao
pg 1147; DOI:
10.1039/P19930001147
PDF
Phenolic constituents of Glycyrrhiza species. Part 10. Glyasperin E, a new 3-phenoxychromen-4-one derivative from the roots of Glycyrrhiza aspera
Lu Zeng Toshio Fukai Taro Nomura Ru-Yi Zhang and Zhi-Cen Lou
pg 1153; DOI:
10.1039/P19930001153
PDF
Novel 10-aziridinyl steroids; inhibitors of aromatase
Vincent C. O. Njar Elam Safi J. V. Silverton and Cecil H. Robinson
pg 1161; DOI:
10.1039/P19930001161
PDF
Synthesis and first X-ray structure analysis of a stabilized chiral chlorobismuthine: fixation of molecular geometry induced by the intramolecular coordination of a sulfonyl group
Hitomi Suzuki Toshihiro Murafuji and Nagao Azuma
pg 1169; DOI:
10.1039/P19930001169
PDF
Preparation and reaction of difluorinated malonaldehydic acid derivatives: a new route to functionalized ,-difluorinated esters and amides
Takashi Tsukamoto and Tomoya Kitazume
pg 1177; DOI:
10.1039/P19930001177
PDF
Synthesis of very long chain fatty acid methyl esters
Marcel R. Kling Christopher J. Easton and Alf Poulos
pg 1183; DOI:
10.1039/P19930001183
PDF
Estrogen biosynthesis: 2-hydroxy-19-oxoandrost-4-ene-3,17-dione revisited
Eliahu Caspi H. Ranjith W. Dharmaratne Esther Roitman and Cedric Shackleton
pg 1191; DOI:
10.1039/P19930001191
PDF
Intramolecular Diels–Alder reaction with furans: effect of the substitution pattern reinvestigated
Dipak Prajapati Dipak R. Borthakur and Jagir S. Sandhu
pg 1197; DOI:
10.1039/P19930001197
PDF
Conference diary

pg viih; DOI:
10.1039/P1993000viih
PDF

Issue 11


Front cover

pg X041; DOI:
10.1039/P199300FX041
PDF
Back cover

pg X043; DOI:
10.1039/P199300BX043
PDF
Contents pages

pg P085; DOI:
10.1039/P199300FP085
PDF
Back matter

pg P091; DOI:
10.1039/P199300BP091
PDF
Preparation of 6-oxo-1,6-dihydropyridine-2-carboxylic acid by microbial hydroxylation of pyridine-2-carboxylic acid
Andreas Kiener Rainer Glöckler and Klaus Heinzmann
pg 1201; DOI:
10.1039/P19930001201
PDF
Do metal perchlorates act as a conventional Lewis acid in the allylstannation of aldehydes?
Yutaka Nishigaichi Noriko Nakano and Akio Takuwa
pg 1203; DOI:
10.1039/P19930001203
PDF
Mechanistic pathways for radical ring expansion/aromatisation of steroid C/D models
Stuart P. Green and Donald A. Whiting
pg 1205; DOI:
10.1039/P19930001205
PDF
Pentenyl mannosides in the synthesis of N-acylmannopyranosyl amides: conformational analysis of intermediates
C. Srinivas Rao Andrew J. Ratcliffe and Bert Fraser-Reid
pg 1207; DOI:
10.1039/P19930001207
PDF
Preparation of [4R-3H]NADH, [4R-3H]NADPH and the corresponding 4S-isomers all with substantial specific activities
Koji Ichinose Finian J. Leeper and Alan R. Battersby
pg 1213; DOI:
10.1039/P19930001213
PDF
Alternative synthesis of 6-(3-methoxybenzyl)pyrazin-2(1H)-one. Synthesis of indeno[1,2-b]pyrazin-2-ones. Crystal structures of 5-acetoxy-1-benzyl-4-tert-butoxycarbonyl-6-(3-methoxybenzylidene)piperazin-2-one, 1-benzyl-4-tert-butoxycarbonyl-7-methoxy-1,3,4,4a-tetrahydroindeno[1,2-b]pyrazin-2-one and 1-benzyl-4-tert-butoxycarbonyl-7-methoxy-1,3,4,9-tetrahydroindeno[1,2-b]pyrazin-2-one
David A. Peters Roy L. Beddoes and John A. Joule
pg 1217; DOI:
10.1039/P19930001217
PDF
Selectivity and specificity in substrate binding to proteases: novel hydrolytic reactions catalysed by -chymotrypsin suspended in organic solvents with low water content and mediated by ammonium hydrogen carbonate
Jean-Marc Ricca and David H. G. Crout
pg 1225; DOI:
10.1039/P19930001225
PDF
A practical synthesis of the anti-tumour agent 2-methyl-4-deoxyisopicropodophyllotoxin and related podophyllin analogues
Andrew R. Beard Sarah J. Hazell John Mann and Christopher Palmer
pg 1235; DOI:
10.1039/P19930001235
PDF
Synthesis, bioactivation and anti-HIV activity of the bis(4-acyloxybenzyl) and mono(4-acyloxybenzyl) esters of the 5-monophosphate of AZT
William Thomson Dave Nicholls William J. Irwin Julian S. Al-Mushadani Sally Freeman Abraham Karpas Juraj Petrik Naheed Mahmood and Alan J. Hay
pg 1239; DOI:
10.1039/P19930001239
PDF
Isolation, structural elucidation and conformational analysis of sesquiterpene pyridine alkaloids from Maytenus ebenifolia Reiss. X-Ray molecular structure of ebenifoline W-I
Hideji Itokawa Osamu Shirota Hiroshi Morita Koichi Takeyaa and Yoichi Iitakab
pg 1247; DOI:
10.1039/P19930001247
PDF
Chiral polyhydroxylated tetrahydrothiophene derivatives: novel synthesis and structural elucidation by X-ray crystallography, NMR spectroscopy and molecular mechanics calculations
A. V. Rama Rao K. Ashok Reddy N. R. Srinivas M. K. Gurjar N. Padmaja S. Ramakumar M. A. Viswamitra G. V. T. Swapna B. Jagannadh and A. C. Kunwar
pg 1255; DOI:
10.1039/P19930001255
PDF
The elimination of an alkoxy group in the photo-Graebe–Ullmann conversion of 1-(2,5-dialkoxyphenyl)triazolopyridines into carbolines, and the preparation of -, - and -carboline quinones
Lina K. Mehta John Parrick and Fereshteh Payne
pg 1261; DOI:
10.1039/P19930001261
PDF
Synthesis of the oligosaccharide segment of a novel phenolic glycolipid antigen from Mycobacterium haemophilum
M. K. Gurjar and K. Revathi Reddy
pg 1269; DOI:
10.1039/P19930001269
PDF
Corrigenda
Sachiko Tsukamoto Masami Ishibashi Takuma Sasaki Jun'Ichi Kobayashi D. David Smith David Hopton Kenneth G. Boyd Robert L. Baxter and Robert Ramage
pg 1273; DOI:
10.1039/P19930001273
PDF
Conference diary

pg viij; DOI:
10.1039/P1993000viij
PDF

Issue 12


Front cover

pg X045; DOI:
10.1039/P199300FX045
PDF
Back cover

pg X047; DOI:
10.1039/P199300BX047
PDF
Contents pages

pg P095; DOI:
10.1039/P199300FP095
PDF
Back matter

pg P099; DOI:
10.1039/P199300BP099
PDF
Aza-Wittig rearrangements and cyclizations by transmetallation of N-benzylaminomethylstannanes
Iain Coldham
pg 1275; DOI:
10.1039/P19930001275
PDF
Cycloaddition of nitrile oxides to homochiral vinyl ethers
Andrew N. Boa Susan E. Booth David A. Dawkins Paul R. Jenkins John Fawcett and David R. Russell
pg 1277; DOI:
10.1039/P19930001277
PDF
A new and facile synthesis of 1H-indazoles
Zhong Zhenqi Xu Tongsheng Chen Xiaonai Qui Yuzhu Zhang Zheng and Hu Hongwen
pg 1279; DOI:
10.1039/P19930001279
PDF
Sites of successive bromination of the ambident nucleophiles 2-methoxy-, 2,4-dimethoxy- and 2,4,6-trimethoxy-benzylidenefluorenes and 2,2-dimesityl-1-tert-butylethenol
Bagrat A. Shainyan Irina Eventova and Zvi Rappoport
pg 1281; DOI:
10.1039/P19930001281
PDF
Unimolecular micelles and globular amphiphiles: dendritic macromolecules as novel recyclable solubilization agents
Craig J. Hawker Karen L. Wooley and Jean M. J. Fréchet
pg 1287; DOI:
10.1039/P19930001287
PDF
Stereoselective construction of vicinal diamines. Part 1. Synthesis of fused pyrazines
Barry S. Orlek Gary T. Borrett and Duncan M. Smith
pg 1299; DOI:
10.1039/P19930001299
PDF
Stereoselective construction of vicinal diamines. Part 2. Synthesis of indenopyrazines
Barry S. Orlek and Diane Lightowler
pg 1307; DOI:
10.1039/P19930001307
PDF
Bakers' yeast reductions of -oxopyrrolidinecarboxylates: synthesis of (+)-cis-(2R,3S)-3-hydroxyproline and (–)-(1S,5S)-Geissman–Waiss lactone, a useful precursor to pyrrolizidine alkaloids
Jeremy Cooper Peter T. Gallagher and David W. Knight
pg 1313; DOI:
10.1039/P19930001313
PDF
Similarities and differences between the mesomorphic behaviour of oligomeric macrocyclics and of linear high relative molecular mass polyethers based on 1-(4-hydroxybiphenyl-4-yl)-2-(4-hydroxyphenyl)butane and flexible spacers
Virgil Percec and Masaya Kawasumi
pg 1319; DOI:
10.1039/P19930001319
PDF
Ozonolysis of cyclopentadiene derivatives. Competitive participation of [3 + 2] and [3 + 4] cycloadditions of carbonyl oxide moieties to ,- unsaturated carbonyl groups
Mitsuyuki Mori Hideyuki Yamakoshi Masatomo Nojima Shigekazu Kusabayashi Kevin J. McCullough Karl Griesbaum Petra Krieger-Beck and In-Chan Jung
pg 1335; DOI:
10.1039/P19930001335
PDF
Tailed MnIII-tetraarylporphyrins bearing an axial ligand and/or a carboxylic group: self-consistent catalysts for H2O2 or NaOCl alkene epoxidation
Pier Lucio Anelli Stefano Banfi Francesco Legramandi Fernando Montanari Gianluca Pozzi and Silvio Quici
pg 1345; DOI:
10.1039/P19930001345
PDF
Isovanillyl sweeteners. Synthesis and sweet taste of sulfur heterocycles
Anna Arnoldi Angela Bassoli Lucio Merlini and Enzio Ragg
pg 1359; DOI:
10.1039/P19930001359
PDF
Conference diary

pg vc; DOI:
10.1039/P199300000vc
PDF

Issue 13


Front cover

pg X049; DOI:
10.1039/P199300FX049
PDF
Back cover

pg X051; DOI:
10.1039/P199300BX051
PDF
Contents pages

pg P103; DOI:
10.1039/P199300FP103
PDF
Back matter

pg P109; DOI:
10.1039/P199300BP109
PDF
A new synthesis, of vinyltins by reaction of phosphorus ylides with acyltins
Jean-Baptiste Verlhac HeeAn Kwon and Michel Pereyre
pg 1367; DOI:
10.1039/P19930001367
PDF
Novel (1,3)-bifunctional organophosphorus(III) phosphonylating agents
Vivienne Sum and Terence P. Kee
pg 1369; DOI:
10.1039/P19930001369
PDF
Lewis acid-induced rearrangement of 2,3-epoxy sulfides: regiospecific nucleophilic trapping of thiiranium ion intermediates with nitrogen nucleophiles
Duncan M. Gill Neil A. Pegg and Christopher M. Rayner
pg 1371; DOI:
10.1039/P19930001371
PDF
A 1,2-silicon shift in cyclopropylidenes leading to 1-trialkylsilylcyclopropenes
Mark S. Baird Cynthia M. Dale and Juma'a R. Al Dulayymi
pg 1373; DOI:
10.1039/P19930001373
PDF
Asymmetric synthesis of homochiral syn- and anti-3-phenylisoserine derivatives: a practical strategy for the synthesis of the taxol C-13 side chain
Mark E. Bunnage Stephen G. Davies and Christopher J. Goodwin
pg 1375; DOI:
10.1039/P19930001375
PDF
Concise synthesis of a porphyrin–cyclocholate molecular bowl
Lindsey G. Mackay Richard P. Bonar-Law and Jeremy K. M. Sanders
pg 1377; DOI:
10.1039/P19930001377
PDF
Substituent-directed regioselectivity in the photocycloaddition of 2,3-dimethylbuta-1,3-diene to the benzene ring
Andrew Gilbert and Owain Griffiths
pg 1379; DOI:
10.1039/P19930001379
PDF
Lipase catalysis in the resolution of racemic intermediates of diltiazem synthesis in organic solvents
Liisa T. Kanerva and Oskari Sundholm
pg 1385; DOI:
10.1039/P19930001385
PDF
Reaction of pyrroles with ethyl 2-nitroso- and 2-azo-propenoates, and with ethyl cyanoformate N-oxide: a comparison of the reaction pathways
Thomas L. Gilchrist and Américo Lemos
pg 1391; DOI:
10.1039/P19930001391
PDF
Asymmetric induction in the Diels–Alder reactions of -hydroxy acyl nitroso compounds
Gordon W. Kirby and Muhammad Nazeer
pg 1397; DOI:
10.1039/P19930001397
PDF
Chalcogenation of tetrathiafulvalene (TTF): synthesis of alkylthio-TTF and alkylseleno-TTF derivatives and X-ray crystal structure of ethylenediseleno TTF (EDS-TTF)
Adrian J. Moore Martin R. Bryce Graeme Cooke Gary J. Marshallsay Peter J. Skabara Andrei S. Batsanov Judith A. K. Howard and Stephen T. A. K. Daley
pg 1403; DOI:
10.1039/P19930001403
PDF
Molecular recognition directed self-assembly of supramolecular cylindrical channel-like architectures from 6,7,9,10,12,13,15,16-octahydro-1,4,7,10,13-pentaoxabenzocyclopentadecen-2-ylmethyl 3,4,5-tris(p-dodecyloxybenzyloxy)benzoate
Virgil Percec Gary Johansson James Heck Goran Ungarb and Simon V. Battyb
pg 1411; DOI:
10.1039/P19930001411
PDF
Enantiospecific synthesis of the (4R)-1-azabicyclo[2.2.1]heptane ring system
Peter G. Houghton Guy R. Humphrey Derek J. Kennedy D. Craig Roberts and Stanley H. B. Wright
pg 1421; DOI:
10.1039/P19930001421
PDF
Preparation of 2,3-disubstituted indoles from indole-3-carboxylic acids and amides by -deprotonation
Cheryl D. Buttery Richard G. Jones and David W. Knight
pg 1425; DOI:
10.1039/P19930001425
PDF
A new method for stereoselective homoallylic amine synthesis
Susan K. Armstrong Eric W. Collington Julian G. Knight Alan Naylorb and Stuart Warren
pg 1433; DOI:
10.1039/P19930001433
PDF
Photoinduced molecular transformations. Part 141. New one-step general synthesis of benzofuran-4,7-diones by the regioselective (3 + 2) photoaddition of 2-hydroxy-1,4-benzoquinones with various alkenes
Kazuhiro Kobayashi Yoshikazu Kanno and Hiroshi Suginome
pg 1449; DOI:
10.1039/P19930001449
PDF
Synthesis of mannose 6-phosphate-containing disaccharide threonine building blocks and their use in solid-phase glycopeptide synthesis
Mette K. Christensen Morten Meldal and Klaus Bock
pg 1453; DOI:
10.1039/P19930001453
PDF
Protected-mode synthesis of N-linked glycopeptides: single-step preparation of building blocks as peracetyl glycosylated NFmoc asparagine OPfp esters
Ida Christiansen-Brams Morten Meldal and Klaus Bock
pg 1461; DOI:
10.1039/P19930001461
PDF
A new synthesis of 2,2-disubstituted unsymmetrical biphenyls based on the intramolecular Ullmann coupling reaction utilising salicyl alcohol as a template
Masami Takahashi Tsuyosi Ogiku Kimio Okamura Tadamasa Da-Te Hiroshi Ohmizu Kazuhiko Kondo and Tameo Iwasaki
pg 1473; DOI:
10.1039/P19930001473
PDF
Synthetic studies on tricyclospirodienones; model chemistry for novel mimics of steroid substrates
Owen Hares David Hobbs-Mallyon and Donald A Whiting
pg 1481; DOI:
10.1039/P19930001481
PDF
Milbemycin synthesis: synthesis of a macrocyclic analogue of non-aromatic -milbemycins
Mark J. Hughes and Eric J. Thomas
pg 1493; DOI:
10.1039/P19930001493
PDF
Milbemycin synthesis: asymmetric synthesis of spiroketals from methyl -D-glucopyranoside
Girish Khandekar Gareth C. Robinson Nicholas A. Stacey Eric J. Thomas and Sunil Vather
pg 1507; DOI:
10.1039/P19930001507
PDF
Synthesis and X-ray molecular structures of p-tert-butylcalix[4]arenes with diamide bridges spanning the 1,3-(distal) positions on the lower rim
Volker Böhmer George Ferguson John F. Gallagher Alan J. Lough M. Anthony McKervey Evelyn Madigan Mary B. Moran James Phillips and Graheme Williams
pg 1521; DOI:
10.1039/P19930001521
PDF
Biosynthesis of estrogens. Estr-5(10)-ene-3,17-dione: isolation, metabolism and mechanistic implications
H. Ranjith W. Dharmaratne James. L. Kilgore Esther Roitman Cedric Shackleton and Eliahu Caspi
pg 1529; DOI:
10.1039/P19930001529
PDF
Corrigendum
Martin Mandel and Tomas Hudlicky
pg 1537; DOI:
10.1039/P19930001537
PDF
Conference diary

pg viik; DOI:
10.1039/P1993000viik
PDF

Issue 14


Front cover

pg X053; DOI:
10.1039/P199300FX053
PDF
Back cover

pg X055; DOI:
10.1039/P199300BX055
PDF
Contents pages

pg P113; DOI:
10.1039/P199300FP113
PDF
Back matter

pg P119; DOI:
10.1039/P199300BP119
PDF
Stereoelectronic control of Cope rearrangement energetics through remote double bonds in novel, rigid polycyclic frames
Goverdhan Mehta S. Hari Krishna Reddy Vasantha Pattabhi S. Bhanumathi Animesh Pramanik and Jayaraman Chandrasekhar
pg 1539; DOI:
10.1039/P19930001539
PDF
Regio- and stereo-specific synthesis of cis-()-1-acetoxy-4-(acetoxymethyl)cyclopent-2-ene: a key intermediate in the synthesis of carbocyclic nucleosides and pseudo-ribofuranoses
David M. Hodgson Jason Witherington and Brian A. Moloney
pg 1543; DOI:
10.1039/P19930001543
PDF
Joalin, the first nitrogen-containing xenicane diterpene isolated from a brown seaweed collected off the Senegalese coast
Graziano Guella Ibrahima N'Diaye Giuseppe Chiasera and Francesco Pietra
pg 1545; DOI:
10.1039/P19930001545
PDF
A new approach to cyclopropene fatty acids involving 1,2-deiodination
Mark S. Baird and Brendan Grehan
pg 1547; DOI:
10.1039/P19930001547
PDF
An approach to the synthesis of (–)-lipstatin by Wittig reaction and Lewis acid-promoted [2 + 2] cycloaddition
Jean-Marc Pons Agnés Pommier Joan Lerpiniere and Philip Kocienski
pg 1549; DOI:
10.1039/P19930001549
PDF
A novel synthetic intermediate in -lactam chemistry: an efficient preparation of cis-1,3,4-tris(trimethylsilyl)azetidin-2-one and its transformation into 4-acetoxy-3-alkylideneazetidin-2-ones
Kohji Suda Katsumi Hotoda Fumiaki Iemuro and Toshikatsu Takanami
pg 1553; DOI:
10.1039/P19930001553
PDF
Cyclizations. Part 1. Electrochemical and photochemical reactions of 1-(4-fluorophenyl)-5-(2-halogenophenyl)tetrazoles
Shileen Donnelly James Grimshaw and Jadwiga Trocha-Grimshaw
pg 1557; DOI:
10.1039/P19930001557
PDF
New oxetane-type taxanes from Taxus wallichiana Zucc.
Giovanni Appendino Hasan Çetin Özen Pierluigi Gariboldi Elisabetta Torregiani Bruno Gabetta Rita Nizzola and Ezio Bombardelli
pg 1563; DOI:
10.1039/P19930001563
PDF
Synthesis, enzymatic stability and base-pairing properties of oligothymidylates containing thymidine dimers with different N-substituted guanidine linkages
Frank Vandendriessche Arthur Van Aerschot Martine Voortmans Gerard Janssen Roger Busson An Van Overbeke Walter Van den Bossche Jos Hoogmartens and Piet Herdewijn
pg 1567; DOI:
10.1039/P19930001567
PDF
Conformational studies of natural products. Part 4. Conformation and absolute configuration of cascarosides A, B, C, D
Paolo Manitto Diego Monti Gioyanna Speranza Nadia Mulinacci Francof F. Vincieri Alberto Griffini and Giorgio Pifferi
pg 1577; DOI:
10.1039/P19930001577
PDF
Recoverable chiral sulfoxides for asymmetric synthesis: preparation, regeneration and application to the asymmetric aldol reaction
Roger J. Butlin Ian D. Linney Douglas J. Critcher Mary F. Mahon Kieran C. Molloy and Martin Wills
pg 1581; DOI:
10.1039/P19930001581
PDF
Ozone-mediated nitration of alkylbenzenes and related compounds with nitrogen dioxide
Hitomi Suzuki Takashi Murashima Iku Kozai and Tadashi Mori
pg 1591; DOI:
10.1039/P19930001591
PDF
First total synthesis of ()-peridinin, ()-pyrrhoxanthin and the optically active peridinin
Yumiko Yamano and Masayoshi Ito
pg 1599; DOI:
10.1039/P19930001599
PDF
Regenerable N-alkylamide hydroperoxide for catalytic substrate oxidation
Douglas E. Patton and Russell S. Drago
pg 1611; DOI:
10.1039/P19930001611
PDF
Heterocycles by cycloaddition. Part 11. Dipolar cycloadditions of mesoionic compounds with tropone: peri-selective [4+ 2] and [4+ 6] cycloadditions
Hiroshi Kato Tomoshige Kobayashi Kazuhiko Tokue and Sonoko Shirasawa
pg 1617; DOI:
10.1039/P19930001617
PDF
C-stannylated carbohydrate derivatives, part 5. 1,2:5,6-Di-O-isopropylidene-3-C-(organostannyl)- and -3-C-(phenylstannyl)methyl--D-allofuranose compounds. X-Ray crystal and molecular structure of 1,2:5,6-di-O-isopropylidene-3-C-(triphenylstannylmethyl)--D-allofuranose
Lynne A. Burnett Solange M. S. V. Doidge-Harrison Simon J. Garden R. Alan Howie Oonah J. Taylor and James L. Wardell
pg 1621; DOI:
10.1039/P19930001621
PDF
Naturally occurring linear fused thiazoline-thiazole containing metabolites: total synthesis of (–)-didehydromirabazole A, a cytotoxic alkaloid from blue–green algae
Gerald Pattenden and Stephen M. Thom
pg 1629; DOI:
10.1039/P19930001629
PDF
Synthesis of cyclic amines and allylic sulfides by phenylthio migration of -hydroxy sulfides
Iain Coldham and Stuart Warren
pg 1637; DOI:
10.1039/P19930001637
PDF
Stannyl-cupration of acetylenes and the reaction of the intermediate cuprates with electrophiles as a synthesis of substituted vinylstannanes
Asunciòn Barbero Purificación Cuadrado Ian Fleming Ana M. González Francisco J. Pulido and Rosa Rubio
pg 1657; DOI:
10.1039/P19930001657
PDF
Synthesis of 6-deoxy-6-phenylphosphonoyl-D-fructopyranoses: the first phosphorus-in-the-ring analogues of a ketose
Tadashi Hanaya Ryuji Okamoto Yurij V. Prikhod'ko Margaret-Ann Armour Alan M. Hogg and Hiroshi Yamamoto
pg 1663; DOI:
10.1039/P19930001663
PDF
Mechanism of arylation of nucleophiles by aryllead triacetates. Part 1. Exclusion of a pathway involving aryl free radicals
Jacqueline Morgan and John T. Pinhey
pg 1673; DOI:
10.1039/P19930001673
PDF
Mechanism of arylation of nucleophiles by aryllead triacetates. Part 2. Support for a ligand coupling process and X-ray molecular structure of (p-methoxyphenyl)--methylphenacyllead (IV) diacetate
Jacqueline Morgan Irmi Buys Trevor W. Hambley and John T. Pinhey
pg 1677; DOI:
10.1039/P19930001677
PDF
Studies on steroidal plant-growth regulators. Part 29. Osmium tetroxide-catalysed asymmetric dihydroxylation of the (22E,24R)- and the (22E,24S)-24-alkyl steroidal unsaturated side chain
Liang-Fu Huang Wei-Shan Zhou Li-Qiang Sun and Xin-Fu Pan
pg 1683; DOI:
10.1039/P19930001683
PDF
-Toxin and analogues as peptide models for protein ion channels
Christine M. Bladon Peter Bladon and John A. Parkinson
pg 1687; DOI:
10.1039/P19930001687
PDF
Studies on reactions of nucleoside H-phosphonates with bifunctional reagents. Part 1. Reaction with amino alcohols
Adam Kraszewski Micha Sobkowskia and Jacek Stawiski
pg 1699; DOI:
10.1039/P19930001699
PDF
Photoinduced electron transfer reactions of pentafluoroiodobenzene with aromatic compounds
Qing-Yun Chen and Zhan-Ting Li
pg 1705; DOI:
10.1039/P19930001705
PDF
Conference diary

pg viil; DOI:
10.1039/P1993000viil
PDF

Issue 15


Front cover

pg X057; DOI:
10.1039/P199300FX057
PDF
Back cover

pg X059; DOI:
10.1039/P199300BX059
PDF
Contents pages

pg P123; DOI:
10.1039/P199300FP123
PDF
Back matter

pg P129; DOI:
10.1039/P199300BP129
PDF
Useful Wittig reagents in 1,3-dithiole and tetrathiafulvalene (TTF) chemistry: 2-thioxo- and 2-oxo-1,3-dithiol-4-ylmethyl(triphenyl)phosphonium bromides
Tomasz Nozdryn Jack Cousseau Alain Gorgues Michel Jubault Jesus Orduna Santiago Uriel and Javier Garin
pg 1711; DOI:
10.1039/P19930001711
PDF
Enzyme-assisted preparation of pure alkanedicarboxylic acid monoesters: chain-length dependence of porcine liver esterase (PLE)-catalysed hydrolyses
Mario Lobell and Manfred P. Schneider
pg 1713; DOI:
10.1039/P19930001713
PDF
An isoxazole route to unsaturated -alkoxycarbonyl--diketones
Raymond C. F. Jones Gurdip Bhalay and Paul A. Carter
pg 1715; DOI:
10.1039/P19930001715
PDF
Synthesis of optically active 5-noraristeromycin: enzyme-catalysed kinetic resolution of 9-(4-hydroxycyclopent-2-enyl)purines
Valeria Merlo Fiona J. Reece Stanley M. Roberts Mike Gregson and Richard Storer
pg 1717; DOI:
10.1039/P19930001717
PDF
Thermal rearrangement of 4-iminomethyl-1,2,3-thiadiazoles
Gerrit L'abbé Mikaëla Verbeke Wim Dehaen and Suzanne Toppet
pg 1719; DOI:
10.1039/P19930001719
PDF
Long-range substituent effects on the regioselectivity of one-carbon ring expansion of norbornan-7-ones
Goverdhan Mehta and Faiz Ahmed Khan
pg 1727; DOI:
10.1039/P19930001727
PDF
Organolead-mediated arylation of allyl -ketoesters: a selective synthesis of isoflavanones and isoflavones
Dervilla M. X. Donnelly Jean-Pierre Finet and Bernard A. Rattigan
pg 1729; DOI:
10.1039/P19930001729
PDF
Asymmetric reactions of 8-phenylmenthyl pyruvate with allyltrimethylsilane, silyl enol ethers and ketene silyl acetals
Ming-Yi Chen and Jim-Min Fang
pg 1737; DOI:
10.1039/P19930001737
PDF
Reactivity of cinnamonitriles with 2-cyano- and 2-ethoxycarbonylacetohydrazides: a novel one-step preparation and crystal structure of 3-oxopyrazolo [3,4-b]pyridines
Ali Hadi Nazario Martin Carmen Méndez Margarita Quinteiro Carlos Seoane José L. Soto Armando Albert and Félix H. Cano
pg 1743; DOI:
10.1039/P19930001743
PDF
Direct access to -oxopropyl carbonates from bulky alcohols
Jean Marc Joumier Christian Bruneau and Pierre H. Dixneuf
pg 1749; DOI:
10.1039/P19930001749
PDF
Studies of heterocyclic compounds. Part 31. 4-Alkyl-5-alkylimino-2-1,2,4-thiadiazolines: synthesis and cycloaddition reactions with nitriles in attempts to prepare 3a4-thia-1,3,4,6-tetraazapentalenes
Long-Li Lai Tak-Ho Ngoi David H. Reid Robin H. Nicol and Jane B. Rhodes
pg 1753; DOI:
10.1039/P19930001753
PDF
Hidden axial chirality as a stereodirecting element in reactions involving enol(ate) intermediates. Part 1. Cyclisation reactions of methyl (4R)-3-(2-diazo-3-oxobutanoyl)thiazolidine-4-carboxylate and related compounds
Brian Beagley Michael J. Betts Robin G. Pritchard Anthony Schofield Richard J. Stoodley and Shaheen Vohra
pg 1761; DOI:
10.1039/P19930001761
PDF
Intramolecular oxidative cyclisation of 1-(4-hydroxyaryl)-2-ketoximes 4-HOArCh2C(NOH)R with phenytiodine(III) bis(trifluoroacetate)
Mesut Kaçan Demet Koyuncu and Alexander McKillop
pg 1771; DOI:
10.1039/P19930001771
PDF
New approach to 3-oxygenated carbazoles. Synthesis of hyellazole and 4-deoxycarbazomycin B
Tomomi Kawasaki Yoshinori Nonaka Miki Akahane Noriko Maeda and Masanori Sakamoto
pg 1777; DOI:
10.1039/P19930001777
PDF
Regioselective acylation of methyl -D-glucopyranoside and methyl -D-mannopyranoside by means of bis(2-oxooxazolidin-3-yl)phosphinic chloride (BOP-Cl)
Angelo Liguori Antonio Procopio Giovanni Romeo Giovanni Sindona and Nicola Uccella
pg 1783; DOI:
10.1039/P19930001783
PDF
Aza-analogues of the repeating disaccharide unit of peptidoglycan. Part 2. Enantiospecific synthesis of peptide-derivatised 2-acetamido-4-O-(2acetamido-2-deoxy--D-glucopyranosyl)-3-O-carboxymethyl-1,2,5-trideoxy-1,5-imino-D-glucitol
Stephen F. Moss and Robert Southgate
pg 1787; DOI:
10.1039/P19930001787
PDF
Synthetic approaches towards nucleocidin and selected analogues; anti-HIV activity in 4-fluorinated nucleoside derivatives
Anita R. Maguire Wei-Dong Meng Stanley M. Roberts and Andrew J. Willetts
pg 1795; DOI:
10.1039/P19930001795
PDF
Indolizine studies. Part 2. Synthesis and NMR spectroscopic analysis of 2-substituted indolizines
Moira L. Bode and Perry T. Kaye
pg 1809; DOI:
10.1039/P19930001809
PDF
Direct synthesis of 2,6-disubstituted pyridines from bicyclic ketals
Jong-Gab Jun Hyun Shun Shin and Sung Hoon Kim
pg 1815; DOI:
10.1039/P19930001815
PDF
Short-step stereoselective synthesis of 2,3,22-triacetoxy-23,24-dinor-5-cholan-6-one: key intermediate for the preparation of 24-norbrassinolide, dolicholide and dolichosterone
Braja G. Hazra Vandana S. Pore and Padmakar L. Joshi
pg 1819; DOI:
10.1039/P19930001819
PDF
Corrigendum
James D. White G. Nagabushana Reddy and Gary O. Spessard
pg 1823; DOI:
10.1039/P19930001823
PDF
Conference diary

pg viim; DOI:
10.1039/P1993000viim
PDF

Issue 16


Front cover

pg X061; DOI:
10.1039/P199300FX061
PDF
Back cover

pg X063; DOI:
10.1039/P199300BX063
PDF
Contents pages

pg P133; DOI:
10.1039/P199300FP133
PDF
Back matter

pg P139; DOI:
10.1039/P199300BP139
PDF
A new approach to azapentalenes by an addition–rearrangement sequence: synthesis of fused 1,2,4-thiadiazoles
Gerrit L'abbé Johan Buelens and Wim Dehaen
pg 1825; DOI:
10.1039/P19930001825
PDF
Leaving group placement to control the stereoselective organoiron-based synthesis of regioisomeric tetrahydrophenanthridine derivatives
Alexander McKillop G. Richard Stephenson and Michael Tinkl
pg 1827; DOI:
10.1039/P19930001827
PDF
Stereoselective syntheses of the 14-hydroxy epimers of amphotericin B methyl ester
Benjamin J. Costello Michael J. Driver William S. MacLachlan and Andrew W. Taylor
pg 1829; DOI:
10.1039/P19930001829
PDF
Substitution and Michael reactions of bicyclic tetronic, tetramic and thiotetronic esters
Alberto Bertucco J. Brennan Marco Fachini Sabine Kluge Patrick J. Murphy Francesca Pasutto Raffaella Signorini and Harri Lloyd Williams
pg 1831; DOI:
10.1039/P19930001831
PDF
Facile dimerisation of 3-benzylideneindoline-2-thiones
Andrew M. Thompson Maruta Boyd and William A. Denny
pg 1835; DOI:
10.1039/P19930001835
PDF
Novel cycloadditions of isoquinoline Reissert salts
Andrew W. Bridge Michael B. Hursthouse Christian W. Lehmann David J. Lythgoe and Christopher G. Newton
pg 1839; DOI:
10.1039/P19930001839
PDF
Stereochemical control (E/Z and syn/anti) by the diphenylphosphinoyl group in the synthesis of allylic alcohols by allylic rearrangement and by 1,4-diastereoselective reduction of enones
Jonathan Clayden Eric W. Collington Jason Elliott Stephen J. Martin Andrew B. McElroy Stuart Warren and David Waterson
pg 1849; DOI:
10.1039/P19930001849
PDF
Spongian pentacyclic diterpenes. Stereoselective synthesis of aplyroseol-1, aplyroseol-2 and deacetylaplyroseol-2
Antonio Abad Manuel Arnó M. Luisa Marín and Ramón J. Zaragozá
pg 1861; DOI:
10.1039/P19930001861
PDF
cis-Stereoisomers of -carotene and its congeners in the alga Dunaliella bardawil, and their biogenetic interrelationships
Warren J. Ebenezer and Gerald Pattenden
pg 1869; DOI:
10.1039/P19930001869
PDF
Alkylation of enol ethers obtained by treatment of ,-unsaturated acetals with organopotassium reagents: an inverse polarity approach
Carlo Canepa Cristina Prandi Luca Sacchi and Paolo Venturello
pg 1875; DOI:
10.1039/P19930001875
PDF
A flexible approach to pyrido[4,3-b]carbazoles. The syntheses of 8,10-dimethoxy-5-methyl-, 5,11-dimethoxy-7,10-dimethyl- and 9-fluoro-5,11- dimethylpyrido[4,3-b]carbazoles by variations of the type D route
Robin J. Hall Priyanthi Dharmasena Jeremy Marchant Ana-M. F. Oliveira- Campos Maria-Joao R. P. Queiroz Manuela M. Raposo and Patrick V. R. Shannon
pg 1879; DOI:
10.1039/P19930001879
PDF
Phenolic oxidations with phenyliodonium diacetate
Andrew Pelter and Said M. A. Elgendy
pg 1891; DOI:
10.1039/P19930001891
PDF
S-p-methylbenzyl--phenylcysteine: a potential tool for probing receptor topologies
Gérald Villeneuve John DiMaio Tak Hang Chan and André Michel
pg 1897; DOI:
10.1039/P19930001897
PDF
Studies directed towards total syntheses of the tropoloisoquinoline alkaloids grandirubrine and imerubrine. Part 2. Thermolysis of 8,9-dihydro-2-hydroxy-3,10,11,12-tetra methoxyisoquino[2,1-c][1,2,3]benzotriazin-7-ium chloride: competitive modes of cyclisation leading to the indeno[1,2,3-ij]isoquinoline (azafluoranthene) skeleton
Martin G. Banwell Ernest Hamel Neil K. Ireland Maureen F. Mackay and Algirdas K. Serelis
pg 1905; DOI:
10.1039/P19930001905
PDF
cis-Dihydrocatechols as precursors to highly oxygenated troponoids. Part 2. Regiocontrolled syntheses of stipitatic and puberulic acids
Martin G. Banwell Maree P. Collis Maureen F. Mackay and Sharon L. Richards
pg 1913; DOI:
10.1039/P19930001913
PDF
Reinvestigation on the catalytic isomerisation of carbon–carbon triple bonds
Cheng Guo and Xiyan Lu
pg 1921; DOI:
10.1039/P19930001921
PDF
An antibody with dual catalytic activity
Colin J. Suckling M. Catriona Tedford Laura M. Bence June I. Irvine and William H. Stimson
pg 1925; DOI:
10.1039/P19930001925
PDF
Reaction of dimethyl methylenesuccinate with hydrazine
Marina Vinnikova David Gertner Shmuel Cohen and Albert Zilkha
pg 1931; DOI:
10.1039/P19930001931
PDF
Conference diary

pg viin; DOI:
10.1039/P1993000viin
PDF

Issue 17


Front cover

pg X065; DOI:
10.1039/P199300FX065
PDF
Back cover

pg X067; DOI:
10.1039/P199300BX067
PDF
Contents pages

pg P141; DOI:
10.1039/P199300FP141
PDF
Michael reaction of functionalized chiral cyclanone imines. Enantioselective synthesis of C2-symmetric cis-(1R,6R)-1,6-dimethylbicyclo[4.4.0]decane-3,8-dione
Michel Pfau Ivan Jabin and Gilbert Revial
pg 1935; DOI:
10.1039/P19930001935
PDF
Simple, inexpensive synthesis of oxiranes from carbonyl compounds. Generation of sulfonium ylides from the ternary system methanol–sulfuric acid–dimethyl sulfide
Julie Forrester Ray V. H. Jones Peter N. Preston and Elizabeth S. C. Simpson
pg 1937; DOI:
10.1039/P19930001937
PDF
(2Z,4E)-1,3,6-triacetoxyhexa-2,4-diene a novel Diels–Alder diene precursor of cyclohexanones
Pilar Areces Emilio Román María C. Pozo and José A. Serrano
pg 1939; DOI:
10.1039/P19930001939
PDF
Concise synthesis of CC-1065/duocarmycin pharmacophore using the intramolecular Heck reaction
Takao Sakamoto Yoshinori Kondo Masanobu Uchiyama and Hiroshi Yamanaka
pg 1941; DOI:
10.1039/P19930001941
PDF
Heck reaction of arenediazonium salts: a palladium-catalysed reaction in an aqueous medium
Saumitra Sengupta and Sanchita Bhattacharya
pg 1943; DOI:
10.1039/P19930001943
PDF
Highly functionalised methylenecyclopropanes from cyclopropenes
Mark S. Baird M. Fiona Shortt Helmi H. Hussain and Juma'a R. Al Dulayymi
pg 1945; DOI:
10.1039/P19930001945
PDF
Peptide synthesis: synthesis of the cysteine-containing peptides of biological and pharmaceutical interest, -h-ANF and h-big endothelin
Robert Ramage and Andrew S. J. Stewart
pg 1947; DOI:
10.1039/P19930001947
PDF
Preparation and reactivity of cuprate derivatives of lithium 6-lithiopiperonylate with tricarbonyl(2-methoxycyclohexadienyl)iron(1+) hexafluorophosphate(1–)
Stephen T. Astley and G. Richard Stephenson
pg 1953; DOI:
10.1039/P19930001953
PDF
Utilisation of L-quebrachitol in natural product synthesis. Total synthesis and absolute configuration of (–)-oudemansin X
Noritaka Chida Ken Yamada and Seiichiro Ogawa
pg 1957; DOI:
10.1039/P19930001957
PDF
Lithium benzenetellurolate-induced Reformatsky-type reaction in the presence of cerium trichloride
Shin-ichi Fukuzawa and Katsuhiko Hirai
pg 1963; DOI:
10.1039/P19930001963
PDF
Stereochemistry and mechanisms of the 3-carboxymuconate fungal pathway in Neurospora SY4a
Robert A. Hill Gordon W. Kirby Gary J. O'Loughlin and David J. Robins
pg 1967; DOI:
10.1039/P19930001967
PDF
Novel rearrangements of cyano-stabilised cyclic sulfur ylides, 2-alkyl-1-cyano-3,4-dihydro-1H-2-thionianaphthalen-1-ides: spiro-compound formation and ring expansion reactions
Tadashi Kataoka Masahiro Kataoka Megumi Ikemori Hiroshi Shimizu Mikio Horia and Iwao Miura
pg 1973; DOI:
10.1039/P19930001973
PDF
Vinyl anion equivalents. Part 3. Diastereoselective allylation of 2-phenylseleno-3-trialkylsilyl- and 2-phenylthio-3-(tributylstannyl)cyclopentanone enolates
Shinya Kusuda Yoshio Ueno Tsuneo Hagiwara and Takeshi Toru
pg 1981; DOI:
10.1039/P19930001981
PDF
Ring-closure reactions of alkenyl oximes induced by persulfate anion oxidation of diphenyl diselenide. Formation of 1,2-oxazines and cyclic nitrones
Marcello Tiecco Lorenzo Testaferri Marco Tingoli Luana Bagnoli and Francesca Marini
pg 1989; DOI:
10.1039/P19930001989
PDF
Oxidation of benzotrithiole analogues. Photochemical rearrangement of benzotrithiole 2-oxides to benzotrithiole 1-oxides involving intramolecular oxygen migration
Naoki Yomoji Shouichi Takahashi Shin-ichi Chida Satoshi Ogawa and Ryu Sato
pg 1995; DOI:
10.1039/P19930001995
PDF
Stereoselective alkene synthesis via silicon-directed [2,3]-sigmatropic rearrangements: an approach to leukotrienes
John E. Crawley Aston D. Kaye Gerald Pattenden and Stanley M. Roberts
pg 2001; DOI:
10.1039/P19930002001
PDF
Synthetic and structural studies of key intermediates toward forskolin and/or erigerol. Relative stereochemistry, conformational preferences and stereoselectivity control
José A. Bacigaluppo María I. Colombo Manuel González-Sierra Marcelo D. Preite Juan Zinczuk Edmundo A. Rúveda Helmut Duddeck and Monika Hiegemann
pg 2009; DOI:
10.1039/P19930002009
PDF
3-Hydroxypyrroles and 1H-pyrrol-3(2H)-ones. Part 13. Reactions of methoxymethylene Meldrum's acid with 3-hydroxypyrroles, with 3-methoxypyrroles and with other active substrates, and pyrolytic heterocyclisations of the products
Paul A. Derbyshire Gordon A. Hunter Hamish McNab and Lilian C. Monahan
pg 2017; DOI:
10.1039/P19930002017
PDF
Study of the transamidative ring expansion of N--halogenoalkyl--lactams of alkyl chain lengths 2–12 in liquid ammonia and other liquid amines: syntheses of 7-, 8- and 9-membered 1,5-diaza cyclic ketones, including routes to ()-dihydroperiphylline and ()-celabenzine
Michael J. Begley Leslie Crombie David Haigh Raymond C. F. Jones Steven Osborne and Richard A. B. Webster
pg 2027; DOI:
10.1039/P19930002027
PDF
Synthesis of the alkaloid homaline in () and natural (S,S)-(–) forms, using amination and transamidative ring expansion in liquid ammonia
Leslie Crombie David Haigh Raymond C. F. Jones and Ab.Rasid Mat-Zin
pg 2047; DOI:
10.1039/P19930002047
PDF
Synthesis of the alkaloids hopromine, hoprominol and hopromalinol, using transamidation methods
Leslie Crombie David Haigh Raymond C. F. Jones and Ab. Rasid Mat-Zin
pg 2055; DOI:
10.1039/P19930002055
PDF
Arylation of -(phenylthio)ketones with aryllead(IV) derivatives: application to the synthesis of 2-arylbenzofuran-3(2H)-one derivatives
Dervilla M. X. Donnelly Joshua M. Kielty Antoine Cormons and Jean-Pierre Finet
pg 2069; DOI:
10.1039/P19930002069
PDF
Synthetic application of lithiated tris(methylthio)methane: preparation of aliphatic methyl thiolcarboxylates from the corresponding halides. Convenient synthesis of tris(methylthio)methane
Margherita Barbero Silvano Cadamuro Iacopo Degani Stefano Dughera and Rita Fochi
pg 2075; DOI:
10.1039/P19930002075
PDF
Reactions of dianions of acyclic -enamino ketones with electrophiles. Part 5. Esters: synthesis of pyridin-4-one and pyran-4-one derivatives
Giuseppe Bartoli Marcella Bosco Cristina Cimarelli Renato Dalpozzo Giuseppe Guercio and Gianni Palmieri
pg 2081; DOI:
10.1039/P19930002081
PDF
Intramolecular reaction of the hydrazonyl group with formyl and oxo groups: preparation of pyrazolo[1,5-a]indoles and related pyrazolo compounds
Jing-Kang Shen Hajime Katayama Noriyuki Takatsu and Itsuo Shiro
pg 2087; DOI:
10.1039/P19930002087
PDF
Oxidative addition reactions of -alkenyl nitronate anions
W. Russell Bowman David S. Brown Catherine A. Burns and David Crosby
pg 2099; DOI:
10.1039/P19930002099
PDF
9-(1-Fluoro-5-hydroxypentan-2-yl)-9H-guanine: synthesis and evaluation of antiviral activity
Maureen Lewis T. Brian H. McMurry and Erik De Clercq
pg 2107; DOI:
10.1039/P19930002107
PDF
Specific complexation of glucose with a diphenylmethane-3,3-diboronic acid derivative: correlation between the absolute configuration of mono- and di-saccharides and the circular dichroic activity of the complex
Yutaka Shiomi Miwako Saisho Kazuhiko Tsukagoshi and Seiji Shinkai
pg 2111; DOI:
10.1039/P19930002111
PDF
Glycosylation of phenols: preparation of 1,2-cis and 1,2-trans glycosylated tyrosine derivatives to be used in solid-phase glycopeptide synthesis
Knud J. Jensen Morten Meldal and Klaus Bock
pg 2119; DOI:
10.1039/P19930002119
PDF
Generation and trapping of benzyl radicals from benzyl iodides by cobaloximemediated iodine atom abstractions
Trevor M. Brown Christopher J. Cooksey David Crich Alan T. Dronsfield and Robert Ellis
pg 2131; DOI:
10.1039/P19930002131
PDF
Rearrangement of morphinandienes in methanesulfonic acid
Sándor Berényi Mónika Czirják and Sándor Makleit
pg 2137; DOI:
10.1039/P19930002137
PDF
Conference diary

pg ixa; DOI:
10.1039/P19930000ixa
PDF

Issue 18


Front cover

pg X069; DOI:
10.1039/P199300FX069
PDF
Back cover

pg X071; DOI:
10.1039/P199300BX071
PDF
Contents pages

pg P149; DOI:
10.1039/P199300FP149
PDF
Photocatalysed addition of pyrrolidines to butenolides: a concise synthesis of the pyrrolizidine alkaloid ring system
Elson Santiago de Alvarenga and John Mann
pg 2141; DOI:
10.1039/P19930002141
PDF
Synthesis of allylsilanes from the [2 + 1] insertion reaction of alkenyl Fischer carbene complexes with silanes
Chi Ching Mak and Kin Shing Chan
pg 2143; DOI:
10.1039/P19930002143
PDF
Preparation and X-ray structure of 8,9,19,20-tetra hydrodinaphtho[1,8jk; 1,8-bc][1,5,9,13]tetraselenacyclohexadecine, and its novel ring contraction in concentrated sulfuric acid
Hisashi Fujihara Masayoshi Yabe Megumi Ikemori and Naomichi Furukawa
pg 2145; DOI:
10.1039/P19930002145
PDF
Synthesis of C-4-substituted qinghaosu analogues
Ya-Jing Rong and Yu-Lin Wu
pg 2147; DOI:
10.1039/P19930002147
PDF
Synthesis of steroidal 1,2,4-trioxane as potential antimalarial agent
Ya-Jing Rong and Yu-Lin Wu
pg 2149; DOI:
10.1039/P19930002149
PDF
Nitrile oxide cycloaddition of non-activated alkynes: a novel approach to the synthesis of neuroactive isoxazoles
Paolo Pevarello Raffaella Amici Maristella Colombo and Mario Varasi
pg 2151; DOI:
10.1039/P19930002151
PDF
New synthesis of dialkyl fluoroalkynylphosphonates
Yanchang Shen and Ming Qi
pg 2153; DOI:
10.1039/P19930002153
PDF
A reinvestigation of the reductive ring-opening of a 3-substituted exo-4,5-epoxytricyclo[5.2.1.02,6]dec-8-en-3-ol to the corresponding 3,5-diol
Zhi-Yu Liu and Xin-Jie Chu
pg 2155; DOI:
10.1039/P19930002155
PDF
Synthesis, photochemistry and enzymology of 2-O-(2-nitrobenzyl)-D-glucose, a photolabile derivative of D-glucose
John E. T. Corrie
pg 2161; DOI:
10.1039/P19930002161
PDF
Formation of a new toxic compound, citrinin H1, from citrinin on mild heating in water
Alka Ben Trivedi Mitsuru Hirota Etsushiro Doi and Naofumi Kitabatake
pg 2167; DOI:
10.1039/P19930002167
PDF
Annulation by sequential double Michael reaction; synthesis of decalones and its application to the syntheses of ?-cadinene, khusitone and khusilal
Hisahiro Hagiwara Tsutomu Akama Akihiro Okano and Hisashi Uda
pg 2173; DOI:
10.1039/P19930002173
PDF
Retinoids and related compounds. Part 15. Synthesis and spectral characterization of bicyclic retinals involving the 8–18 or 8–16 bonded structure
Yuko Katsuta Miho Sakai and Masayoshi Ito
pg 2185; DOI:
10.1039/P19930002185
PDF
Catalytic enantio- and diastereo-selective addition of diethylzinc to racemic -thio- and -seleno-aldehydes: asymmetric synthesis of optically active vicinal thio- and seleno-alcohols
Makoto Watanabe Mineo Komota Masamichi Nishimura Shuki Araki and Yasuo Butsugan
pg 2193; DOI:
10.1039/P19930002193
PDF
Photochemical reactions of benzothiazole-2-thiones
Takehiko Nishio Yo-ichi Mori and Akira Hosomi
pg 2197; DOI:
10.1039/P19930002197
PDF
Remarkable orientational effects in the displacement of the fluorine from heptafluoro-isoquinoline and -quinoline towards sulfur nucleophiles. Further reactions with oxygen nucleophiles
Gerald M. Brooke Richard D. Chambers Christopher J. Drury and Michael J. Bower
pg 2201; DOI:
10.1039/P19930002201
PDF
Evaluation of through-space interaction in [2.2]metacyclophanes by diazo coupling reaction
Akihiko Tsuge Tetsuji Moriguchi Shuntaro Mataka and Masashi Tashiro
pg 2211; DOI:
10.1039/P19930002211
PDF
Photochemical transformation of bufadienolide into 14,21-epoxycholanes via photolytic methanolysis
Takahiro Tanase Nobutoshi Murakami Akito Nagatsu and Jinsaku Sakakibara
pg 2217; DOI:
10.1039/P19930002217
PDF
Stereoselective synthesis of ()-veadeiroic acid and ()-veadeirol by cyclisation of a 2-(2-arylethyl)-1,3,3-trimethylcyclohexyl cation: mechanism and stereochemistry of related cycloalkylation reactions
Arabinda Saha and Dhanonjoy Nasipuri
pg 2223; DOI:
10.1039/P19930002223
PDF
Synthesis of 4-alkylpyrazoles from 3,5-diaminopyrazoles
Aurea Echevarría José Elguero Gloria I. Yranzo Enrique Diez-Barra Antonio de la Hoz Andrés Moreno and Miguel Angel García-Martín
pg 2229; DOI:
10.1039/P19930002229
PDF
Evidence for a new pathway in the microbial conversion of 3-acetoxycholest-5-en-19-ol into estrone
V. N. Shankar T. N. Guru Row and K. M. Madyastha
pg 2233; DOI:
10.1039/P19930002233
PDF
Conference diary

pg viio; DOI:
10.1039/P1993000viio
PDF

Issue 19


Front cover

pg X073; DOI:
10.1039/P199300FX073
PDF
Back cover

pg X075; DOI:
10.1039/P199300BX075
PDF
Contents pages

pg P155; DOI:
10.1039/P199300FP155
PDF
Back matter

pg P161; DOI:
10.1039/P199300BP161
PDF
Rapid enantioselective access to des-AB-trienic corticosteroids via intramolecular cycloaddition
Hideo Nemoto Atsushi Satoh and Keiichiro Fukumoto
pg 2237; DOI:
10.1039/P19930002237
PDF
1 H-cyclopropa(b)naphthalene-3,6-dione
Brian Halton Andrew J. Kay and Zha Zhi-mei
pg 2239; DOI:
10.1039/P19930002239
PDF
Efficient asymmetric synthesis of indolizidine building blocks
Timothy J. Bond Robert Jenkins Andrew C. Ridley and Paul C. Taylor
pg 2241; DOI:
10.1039/P19930002241
PDF
Synthesis of a new class of asymmetric ketone reduction catalyst via a diastereoselective cyclisation reaction: X-ray crystal structure of S(p)R-(–)-N-(tert-butyldiphenylsilyl)dihydrobenzazaphosphole oxide
Barry Burns Eric Merifield Mary F. Mahon Kieran C. Molloy and Martin Wills
pg 2243; DOI:
10.1039/P19930002243
PDF
Microbial generation of (2R,3S)- and (2S,3S)-ethyl 2-benzamidomethyl-3-hydroxybutyrate, a key intermediate in the synthesis of (3S,1R)-3-(1-hydroxyethyl)azetidin-2-one
Claudio Fuganti Simonetta Lanati Stefano Servi Auro Tagliani Angelo Bedeschi and Giovanni Franceschi
pg 2247; DOI:
10.1039/P19930002247
PDF
Deconjugation of ,-unsaturated esters and an intramolecular Michael reaction of bis-,-unsaturated esters with trialkylsilyl trifluoromethanesulfonate in the presence of tertiary amine: synthesis of ()-ricciocarpin A
Masataka Ihara Shuichi Suzuki Nobuaki Taniguchi and Keiichiro Fukumoto
pg 2251; DOI:
10.1039/P19930002251
PDF
Synthesis and thermolysis of 5-azido-4-formyloxazoles
Gerrit L'Abbé Anna-Maria Ilisiu Wim Dehaen and Suzanne Toppet
pg 2259; DOI:
10.1039/P19930002259
PDF
Alkylation of 4H,6H-thieno[3,4-c]furan 5,5-dioxide and its use as a 3,4-dimethylenefuran synthon in intramolecular Diels–Alder reaction
Kaori Ando Naoki Akadegawa and Hiroaki Takayama
pg 2263; DOI:
10.1039/P19930002263
PDF
[3 + 2]-Annulation using allylidene(triphenyl)phosphoranes: a one-step synthesis of cyclopentadienes
Minoru Hatanaka Yuichiro Himeda and Ikuo Ueda
pg 2269; DOI:
10.1039/P19930002269
PDF
Electrophilic ene-type reactions of phenyl vinyl sulfoxide with alkenes
Jeremy Harvey Marie-Hélène Brichard and Heinz G. Viehe
pg 2275; DOI:
10.1039/P19930002275
PDF
Strain-assisted reductive ring cleavage: convenient route to bridged eight-membered rings present in taxanes
Subrata Ghosh Subrata Sarkar and Goutam Saha
pg 2281; DOI:
10.1039/P19930002281
PDF
Some diastereoselective enzyme-catalysed esterifications and interesterifications
Emma L. A. Macfarlane Stanley M. Roberts Veronique G. R. Steukers and Philip L. Taylor
pg 2287; DOI:
10.1039/P19930002287
PDF
Phosphotriester approach to the synthesis of oligonucleotides: a reappraisal
Colin B. Reese and Zhang Pei-Zhuo
pg 2291; DOI:
10.1039/P19930002291
PDF
Synthesis and bioactivation of bis(aroyloxymethyl) and mono(aroyloxymethyl) esters of benzylphosphonate and phosphonoacetate
William Thomson Dave Nicholls Antony G. Mitchell Julie A. Corner William J. Irwin and Sally Freeman
pg 2303; DOI:
10.1039/P19930002303
PDF
Biosynthetic studies on virginiae butanolide A, a butyrolactone autoregulator from Streptomyces. Part 2. Preparation of possible biosynthetic intermediates and conversion experiments in a cell-free system
Shohei Sakuda Sumiko Tanaka Kimihiro Mizuno Oratai Sukcharoen Takuya Nihira and Yasuhiro Yamada
pg 2309; DOI:
10.1039/P19930002309
PDF
Isolation of episulfones from the Ramberg–Bcklund rearrangement. Part 2. X-Ray molecular structure of 2,3-epithio-8,8-dimethyl-6,10- dioxaspiro[4.5]decane S,S-dioxide and of r-6-benzyl-t-7,t-8-epithio-1,4-dioxaspiro[4.4]nonane S,S-dioxide
Stephen M. Jeffery Alan G. Sutherland Simon M. Pyke Aanne K. Powell and Richard J. K. Taylor
pg 2317; DOI:
10.1039/P19930002317
PDF
Chiral cyclobutanones as versatile synthons: the first enantioselective total synthesis of (+)-laurene
Hideo Nemoto Masatoshi Nagamochi and Keiichiro Fukumoto
pg 2329; DOI:
10.1039/P19930002329
PDF
Synthesis based on cyclohexadienes. Part 8. Synthesis of 1-methylbicyclo[2.2.2]oct-2-enecarboxylate derivatives
G. S. R. Subba Rao and K. Vijaya Bhaskar
pg 2333; DOI:
10.1039/P19930002333
PDF
Indirect electroreductive cyclisation of N-allylic and N-propargylbromo amides and o-bromoacryloylanilides using nickel(II) complexes as electron-transfer catalysts
Shigeko Ozaki Hidenori Matsushita and Hidenobu Ohmori
pg 2339; DOI:
10.1039/P19930002339
PDF
Reactions of tetrasulfur tetranitride with alkyl aryl ketoximes: synthesis of 3-aryl- and 3-alkyl-4-aryl-1,2,5-thiadiazoles
Jaeeock Cho and Kyongtae Kim
pg 2345; DOI:
10.1039/P19930002345
PDF
Autoxidation study of carotane sesquiterpenes possessing a non-conjugated 1,4-diene system
Yasuyuki Hashidoko Satoshi Tahara and Junya Mizutani
pg 2351; DOI:
10.1039/P19930002351
PDF
Preparation of optically active amines by a combination of Gabriel synthesis and optical resolution. X-Ray crystal structure of the adduct between (–)-10,10-dihydroxy-9,9-biphenanthryl and N-(1-tert-butyl-2-oxoazetidin-3-yl)phthalimide
Fumio Toda Shinichi Soda and Israel Goldberg
pg 2357; DOI:
10.1039/P19930002357
PDF
Novel molecules for the design of organic conductors. Synthesis of 7,7,8,8-tetracyano-2,5-bis(3-phenylpropyl)-p-quinodimethane and N,N-dicyano-2,5-bis(3-phenylpropyl)-p-quinodiimine and X-ray structure of the TCNQ derivative
Nazario Martin José Luis Segura Carlos Seoane Armando Albert and Félix H. Cano
pg 2363; DOI:
10.1039/P19930002363
PDF
Use of the chlorophyll derivative, purpurin-18, for syntheses of sensitizers for use in photodynamic therapy
Shwn-Ji H. Lee Nadine Jagerovic and Kevin M. Smith
pg 2369; DOI:
10.1039/P19930002369
PDF
Conference diary

pg viip; DOI:
10.1039/P1993000viip
PDF

Issue 20


Front cover

pg X077; DOI:
10.1039/P199300FX077
PDF
Back cover

pg X079; DOI:
10.1039/P199300BX079
PDF
Contents pages

pg P163; DOI:
10.1039/P199300FP163
PDF
Back matter

pg P169; DOI:
10.1039/P199300BP169
PDF
Synthesis and biological activity of stereochemically locked derivatives of jasmonic acid
Jane L. Ward and Michael H. Beale
pg 2379; DOI:
10.1039/P19930002379
PDF
Arylation of 4-ethoxycarbonyl-2-phenyloxazol-5-one by aryllead triacetates: a convenient route to -arylglycines
Mark J. Koen Jacqueline Morgan and John T. Pinhey
pg 2383; DOI:
10.1039/P19930002383
PDF
Dicyanomethylenethiiranes from thioketenes and tetracyanoethylene oxide
Gunadi Adiwidjaja Oliver Bolte Bettina Dietz and Ernst Schaumann
pg 2385; DOI:
10.1039/P19930002385
PDF
A novel approach to functionalised polycyclic systems; intramolecular Diels–Alder reactions of 2-acylated derivatives of 4H,6H-thieno[3,4-c]furan 5,5-dioxide
Takaaki Hayashi Yoh Kawakami Katsuhiro Konno and Hiroaki Takayama
pg 2387; DOI:
10.1039/P19930002387
PDF
Polymerisation of 10-hydroxydecanoic acid with the lipase from Candida cylindracea
David O'Hagan and Naveed A. Zaidi
pg 2389; DOI:
10.1039/P19930002389
PDF
1,3-Dipolar cyctoadditions of 4,5-dihydroimidazolium ylides: new protocols for the synthesis of pyrrolidines and pyrrolo[1,2-a]pyrazines
Raymond C. F. Jones and Kevin J. Howard
pg 2391; DOI:
10.1039/P19930002391
PDF
Intramolecular Diels–Alder reactions of vinylfurans leading to furanodecalins
Philip Cornwall Colin P. Dell and David W. Knight
pg 2395; DOI:
10.1039/P19930002395
PDF
Enzymatic acylation in the resolution of methyl threo-2-hydroxy-3-(4-methoxyphenyl)-3-(2-X-phenylthio)propionates in organic solvents
Liisa T. Kanerva and Oskari Sundholm
pg 2407; DOI:
10.1039/P19930002407
PDF
Unexpected formation of triarylbismuth diformates in the oxidation of triarylbismuthines with ozone at low temperatures
Hitomi Suzuki Tohru Ikegami Yoshihiro Matanoa and Nagao Azuma
pg 2411; DOI:
10.1039/P19930002411
PDF
Radical decarboxylative alkylation onto heteroaromatic bases with trivalent iodine compounds
Hideo Togo Masahiko Aoki Tadashi Kuramochi and Masataka Yokoyama
pg 2417; DOI:
10.1039/P19930002417
PDF
Novel, regioselective allylamine construction; first synthesis of geranyllinaloisocyanide, a diterpene from the marine sponge, Halichondria sp.
Yoshiyasu Ichikawa Masatugu Yamazaki and Minoru Isobe
pg 2429; DOI:
10.1039/P19930002429
PDF
A study of the ferrous ion-initiated SRN1 reactions of halogenoarenes with tert-butyl acetate and N-acylmorpholine enolates
Milco van Leeuwen and Alexander McKillop
pg 2433; DOI:
10.1039/P19930002433
PDF
Donor–acceptor accelerated norbornadiene rearrangements
Christine Bleasdale and David W. Jones
pg 2441; DOI:
10.1039/P19930002441
PDF
Synthesis of optically active amides from -furyl and -phenyl esters by way of enzymatic aminolysis
Vicente Gotor Emma Menéndez Zephirin Mouloungui and Antoine Gaset
pg 2453; DOI:
10.1039/P19930002453
PDF
Complexation and photoinduced electron-transfer reaction between perfluoroalkyl iodides and N,N,N,N-tetramethylphenylene-1,4-diamine, anilines and piperazines
Qing-Yun Chen Zhan-Ting Li and Cheng-Min Zhou
pg 2457; DOI:
10.1039/P19930002457
PDF
An expeditious synthesis of 3-alkyl-, aryl- and heteroaryl-indoles by way of an intramolecular Horner–Wittig reaction
Axel Couture Eric Deniau Yves Gimbert and Pierre Grandclaudon
pg 2463; DOI:
10.1039/P19930002463
PDF
Oligomeric flavanoids. Part 16. Novel prorobinetinidins and the first A-type proanthocyanidin with a 5-deoxy A- and a 3,4-cis C-ring from the maiden investigation of commercial wattle bark extract
Annemarie Cronjé Jan P. Steynberg E. Vincent Brandt Desmond A. Young and Daneel Ferreira
pg 2467; DOI:
10.1039/P19930002467
PDF
Reaction of 4-phenylbut-3-en-2-one with cyanoacetamide in 2 : 1 ratio
Conor N. O'Callaghan T. Brian H. McMurry Christine J. Cardin and Deborah J. Wilcock
pg 2479; DOI:
10.1039/P19930002479
PDF
A facile one-step synthesis of aromatic indolizines by 1,3-dipolar cycloaddition of pyridinium and related heteroaromatic ylides with alkenes in the presence of TPCD [Copy4(HCrO4)2]
Xudong Wei Yuefei Hu Tingsheng Li and Hongwen Hu
pg 2487; DOI:
10.1039/P19930002487
PDF
Copper(II)-catalyzed molecular rearrangements: the behaviour of arylhydrazones of some 3-benzoylazoles in the presence of copper(II) acetate
Silvestre Buscemi Vincenzo Frenna Nicolò Vivona and Domenico Spinelli
pg 2491; DOI:
10.1039/P19930002491
PDF
Optically active tricarbonyl(6-o-trimethylsilylbenzaldehyde)chromium(O) complexes in organic synthesis: a highly diastereoselective 1,3-dipolar cycloaddition with electron-rich olefins
Chisato Mukai In Jong Kim Won Jea Cho Masaru Kido and Miyoji Hanaoka
pg 2495; DOI:
10.1039/P19930002495
PDF
Conference diary

pg viiq; DOI:
10.1039/P1993000viiq
PDF

Issue 21


Front cover

pg X081; DOI:
10.1039/P199300FX081
PDF
Back cover

pg X083; DOI:
10.1039/P199300BX083
PDF
Contents pages

pg P171; DOI:
10.1039/P199300FP171
PDF
Syntheses of conduritol D derivatives from aromatic compounds
Howard A. J. Carless Kofi Busia Yvonne Dove and Shahnaz S. Malik
pg 2505; DOI:
10.1039/P19930002505
PDF
Unusual chemo- and stereo-selectivities in the reactions of 1,2-dichlorocyclopropenes with nitrile oxides
Mark S. Baird Xiaoming Li Juma'a R. Al Dulayymi Alexander I. Kurdjukov and Valery A. Pavlov
pg 2507; DOI:
10.1039/P19930002507
PDF
Unprecedented route to enolates from silyl enol ethers and enol acetates: reaction with hard and soft electrophiles
Pierre Duhamel Dominique Cahard and Jean-Marie Poirier
pg 2509; DOI:
10.1039/P19930002509
PDF
Investigation of the potential of molybdenum(VI) hydrazido(2–) complexes as sources of nitrenium ions: cleavage of the N–N bond and incorporation of the -nitrogen group into solvent molecules
Marc M. Baum and Edward H. Smith
pg 2513; DOI:
10.1039/P19930002513
PDF
Diamide analogues of phosphatidyl choline as potential anti-AIDS agents
Chunhua Jia and Alan H. Haines
pg 2521; DOI:
10.1039/P19930002521
PDF
Biosynthetic relationships in the desertomycin family
Marion Mayer and Ralf Thiericke
pg 2525; DOI:
10.1039/P19930002525
PDF
Synthesis of podophyllum lignans via an isolable o-quinonoid pyrone
David W. Jones and Adrian M. Thompson
pg 2533; DOI:
10.1039/P19930002533
PDF
Synthesis of ()-4-deoxypodophyllotoxin, ()-podophyllotoxin and ()-epipodophyllotoxin
David W. Jones and Adrian M. Thompson
pg 2541; DOI:
10.1039/P19930002541
PDF
Synthesis of 3-octyl-, 3-cyclohexylmethyl- and 3-carboxy-3-(prop-2-ynyl)pyrrolidine-2,5-diones required as potential aromatase inhibitors
Lawrence W. L. Woo H. John Smith Kevin J. Barrell and Paul J. Nicholls
pg 2549; DOI:
10.1039/P19930002549
PDF
Purines, pyrimidines and imidazoles. Part 67. Some N-substituted o-(2-hydroxyethyl)benzyl-purines, -pyrimidines and -imidazoles as aromatic acylonucleoside analogues
Demetrios C. Agathocleous and Gordon Shaw
pg 2555; DOI:
10.1039/P19930002555
PDF
Synthesis of the naturally occurring indolequinone BE 10988, an inhibitor of topoisomerase II
Christopher J. Moody and Elizabeth Swann
pg 2561; DOI:
10.1039/P19930002561
PDF
The synthesis of 5-ylidenepyrrol-2(5H)-ones from maleimides and from pyrrol-2-(5H)-ones
G. Bryon Gill Gwyn D. James Karen V. Oates and Gerald Pattenden
pg 2567; DOI:
10.1039/P19930002567
PDF
Total synthesis of pukeleimide A, a 5-ylidenepyrrol-2(5H)-one from blue green algae
Gwyn D. James Stuart D. Mills and Gerald Pattenden
pg 2581; DOI:
10.1039/P19930002581
PDF
Synthesis of deoxydinucleoside phosphates containing 6-thio-substituted purine nucleobases
Pascale Clivio Jean-Louis Fourrey and Alain Favre
pg 2585; DOI:
10.1039/P19930002585
PDF
Synthetic modulation of the peripheral 2-, 3-, 9- and 12-oxygenation pattern of rotenoids
Leslie Crombie and Jonathan L. Josephs
pg 2591; DOI:
10.1039/P19930002591
PDF
Rotenoid synthesis by Wadsworth–Emmons coupling and Mukaiyama cyclisation: application to 5-thiorotenoids
Leslie Crombie and Jonathan L. Josephs
pg 2599; DOI:
10.1039/P19930002599
PDF
Synthesis of trans-B/C-rotenoids: X-ray and NMR data for cis- and trans-forms of isorotenone
Michael J. Begley Leslie Crombie Hamid Bin A. Hadi and Jonathan L. Josephs
pg 2605; DOI:
10.1039/P19930002605
PDF
Reaction of N-unsubstituted imidazoles with benzonitrile oxide
Giovanni Grassi Francesco Foti Francesco Risitano Giuseppe Bruno Francesco Nicolo and Giovanni De Munno
pg 2615; DOI:
10.1039/P19930002615
PDF
Asymmetric synthesis of dibenzylbutyrolactones and aryltetralin lignan lactones by tandem conjugate addition to a chiral butenolide
Andrew Pelter Robert S. Ward D. Martin Jones and Peter Maddocks
pg 2621; DOI:
10.1039/P19930002621
PDF
Asymmetric synthesis of lignans of the dibenzylbutanediol and tetrahydrodibenzocyclooctene series
Andrew Palter Robert S. Ward D. Martin Jones and Peter Maddocks
pg 2631; DOI:
10.1039/P19930002631
PDF
Convenient synthesis of alcohol O-hemiesters using isopropenyl esters as acylating reagents: synthesis of hydrophilic oxaunomycin 10-O-hemiester derivatives
Yasuyuki Kita Hiroshi Maeda Fumie Takahashi and Seiji Fukui
pg 2639; DOI:
10.1039/P19930002639
PDF
Bicycloannulation of -bromo ,-unsaturated esters; synthesis of the tricyclo[4.4.0.01,5]decane framework and its congeners
Hisashiro Hagiwara Futoshi Abe and Hisashi Uda
pg 2651; DOI:
10.1039/P19930002651
PDF
Synthesis of 5-(acylethynyl)uracils and their corresponding 2-deoxyribonucleosides through palladium-catalysed reactions
Nitya G. Kundu and Swapan K. Dasgupta
pg 2657; DOI:
10.1039/P19930002657
PDF
Conference diary

pg viir; DOI:
10.1039/P1993000viir
PDF

Issue 22


Front cover

pg X085; DOI:
10.1039/P199300FX085
PDF
Back cover

pg X087; DOI:
10.1039/P199300BX087
PDF
Contents pages

pg P177; DOI:
10.1039/P199300FP177
PDF
Selective synthesis of oximes with primary aliphatic amines and hydrogen peroxide in the presence of catalytic quantities of titanium silicalite molecular sieves
J. Sudhakar Reddy and Pierre A. Jacobs
pg 2665; DOI:
10.1039/P19930002665
PDF
Synthesis and nuclease activity of some porphyrin–acridone hybrid molecules
Goverdhan Mehta Thota Sambaiah Bhaskar G. Maiya Mallena Sirish and Dipankar Chatterjee
pg 2667; DOI:
10.1039/P19930002667
PDF
Stapled calix[n]arenes: immobilization of the calix[4]arene conformation by cross-linking on the upper rim
Atsushi Ikeda and Seiji Shinkai
pg 2671; DOI:
10.1039/P19930002671
PDF
Double-bond migration in pyrano[4,3-b]pyrylium cations
Francis M. Dean Malak Malki and Luke J. O'Keeffe
pg 2675; DOI:
10.1039/P19930002675
PDF
The synthesis of radiosensitizers designed to bind to the minor groove of duplex DNA
John Parrick Manuchehr Porssa and Terence C. Jenkins
pg 2681; DOI:
10.1039/P19930002681
PDF
Synthesis of functionalized 1-silyl-substituted dienes by regioselective cyclopropanation of 1-silyl-substituted butadienes with dibromocarbene followed by AgI-promoted ring-opening of the resulting dibromocyclopropanes
Wu-Wang Weng and Tien-Yau Luh
pg 2687; DOI:
10.1039/P19930002687
PDF
Synthesis of 2-substituted buta-1,3-dienes from 1,4-dichlorobut-2-yne via organoboranes
Masayuki Hoshi and Akira Arase
pg 2693; DOI:
10.1039/P19930002693
PDF
Synthetic, stereochemical and mechanistic studies on the asymmetric phosphonylation of aldehydes via 2-triorganosiloxy-1,3,2-oxazaphospholidines
Vivienne Sum and Terence P. Kee
pg 2701; DOI:
10.1039/P19930002701
PDF
Structures of the pyrazines from the mandibular gland secretion of the ponerine ant Dinoponera australis
Neil J. Oldham and E. David Morgan
pg 2713; DOI:
10.1039/P19930002713
PDF
A versatile new method for structure determination in hyperbranched macromolecules
Peter Kambouris and Craig J. Hawker
pg 2717; DOI:
10.1039/P19930002717
PDF
Secondary mould metabolites: Part 45. Isolation and structure elucidation of sulcatine G, a novel sesquiterpene from Laurilia sulcata
Alberto Arnone Gianluca Nasini and Orso Vajna de Pava
pg 2723; DOI:
10.1039/P19930002723
PDF
Potassium tert-butoxide-catalysed oxygenations of vitamin E and its model compound 2,2,5,7,8-pentamethylchroman-6-ol
Shigenobu Matsumoto Yoichi Iitaka Shun-ichiro Nakano and Mitsuyoshi Matsuo
pg 2727; DOI:
10.1039/P19930002727
PDF
Stereoselective addition of nitromethane to levoglucosenone; formation and structure of 2 : 1 and 1 : 2 adducts
Angus C. Forsyth Robert O. Gould R. Michael Paton Ian H. Sadler and Ian Watt
pg 2737; DOI:
10.1039/P19930002737
PDF
Synthesis of medium ring ethers. Part 4. Stereoselective Claisen-mediated ring expansion as a route to homochiral disubstituted medium ring lactones
Mary Ann M. Fuhry Andrew B. Holmes and David R. Marshall
pg 2743; DOI:
10.1039/P19930002743
PDF
2,4-Dihalogenoquinolines. Synthesis, orientation effects and 1H and 13C NMR spectral studies
Alan G. Osborne Jill M. Buley Helen Clarke Rachel C. H. Dakin and Paul I. Price
pg 2747; DOI:
10.1039/P19930002747
PDF
New entry to the imidazo[4,5-c]pyrazole system through photochemically induced sequential transformations of substituted pyrrolo[2,3-d]-1,2,3-triazoles: X-ray crystal structure of a substituted 1,3a,6,6a-tetrahydroimidazo[4, 5-c] pyrazole
Richard N. Butler David M. Colleran Donal F. O'Shea Desmond Cunningham Patrick McArdle and Ann M. Gillan
pg 2757; DOI:
10.1039/P19930002757
PDF
Synthesis of 1,3-disubstituted-pyrrolo[2,1-a]isoquinoline-2-carboxylic acids, esters and amides
Andrew W. Bridge Garry Fenton Frank Halley Michael B. Hursthouse Christian W. Lehmann and David J. Lythgoe
pg 2761; DOI:
10.1039/P19930002761
PDF
High pressure organic chemistry. Part 17. Diels–Alder reaction of methyl palustrate with maleic anhydride and N-phenylmaleimide
Hiyoshizo Kotsuki Masanori Kataoka Kohtaro Matsuo Shigeru Suetomo Motoo Shiroc and Hitoshi Nishizawa
pg 2773; DOI:
10.1039/P19930002773
PDF
Pyridoxal derivatives as probes for water concentration in non-aqueous solvents
Linda Brown Grant A. Johnston Colin J. Suckling Peter J. Halling and Rao H. Valivety
pg 2777; DOI:
10.1039/P19930002777
PDF
Photochemical reaction of 3-hydroxy-1-(o-methylaryl)alkan-1-ones: formation of cyclopropane-1,2-diols and benzocyclobutenols through - and -hydrogen abstractions
Michikazu Yoshioka Satoru Miyazoea and Tadashi Hasegawa
pg 2781; DOI:
10.1039/P19930002781
PDF
Trifluoromethylated furans via iodocyclisation of -unsaturated ethyl trifluoroacetoacetates
Jean-Pierre Bégué Danièle Bonnet-Delpon Romain Dogbeavou and Michèle Ourévitch
pg 2787; DOI:
10.1039/P19930002787
PDF
Reactions of N-cinnamoylaziridines by generation of aziridino ketyls from homolytic cleavage of Michael adducts
Gunther Bentz Jürgen Werry and Helmut Stamm
pg 2793; DOI:
10.1039/P19930002793
PDF
Self-assembly of taper-shaped monoesters of oligo(ethylene oxide) with 3,4,5-tris(p-dodecyloxybenzyloxy)benzoic acid and of their polymethacrylates into tubular supramolecular architectures displaying a columnar mesophase
Virgil Percec James Heck Dimitris Tomazos Frederick Falkenberg Helen Blackwell and Goran Ungar
pg 2799; DOI:
10.1039/P19930002799
PDF
Synthesis based on cyclohexadienes. Part 9. Total synthesis of ()-seychellene
G. S. R. Subba Rao and K. Vijaya Bhaskar
pg 2813; DOI:
10.1039/P19930002813
PDF
Fully regiocontrolled synthesis of ()-12a, 12b-secocolchicine and studies concerning its cyclisation to the alkaloid colchicine
Martin G. Banwell John N. Lambert and G. Lance Gravatt
pg 2817; DOI:
10.1039/P19930002817
PDF
Preparation of key intermediates for the asymmetric synthesis of oxygenated elemanoids
Michiharu Kato Fusao Kido Masataka Watanabe Yoshiaki Masuda and Bahlul Z. Awen
pg 2831; DOI:
10.1039/P19930002831
PDF
Photoinduced molecular transformations. Part 143. (2 + 2) Photoaddition of 3-hydroxy-1-benzopyran-2-one, 3-benzyloxycarbonyloxy-1-benzopyran-2-one, and their 8-methoxy derivatives, with alkenes and formation of 1,2-disubstituted 1,2-dihydrofuro[2,3-c][1]benzopyran-4-ones by way of -scission of cyclobutanoxyl radicals generated from the resulting [2 + 2] photoadducts
Kazuhiro Kobayashi Masayoshi Suzuki and Hiroshi Suginome
pg 2837; DOI:
10.1039/P19930002837
PDF
Synthesis of azapeptides by the Fmoc/tert-butyl/polyamide technique
Martin Quibell William G. Turnell and Tony Johnson
pg 2843; DOI:
10.1039/P19930002843
PDF
Effect of alkene structure on the course of reactions with XeF2 and CsSO4F
Marko Zupan Maja Metelko and Stojan Stavber
pg 2851; DOI:
10.1039/P19930002851
PDF
Conference diary

pg ixb; DOI:
10.1039/P19930000ixb
PDF

Issue 23


Front cover

pg X089; DOI:
10.1039/P199300FX089
PDF
Back cover

pg X091; DOI:
10.1039/P199300BX091
PDF
Contents pages

pg P185; DOI:
10.1039/P199300FP185
PDF
O-Bridged medium sized rings via bicyclic oxonium ylides
F. G. West T. H. Eberlein and Richland W. Tester
pg 2857; DOI:
10.1039/P19930002857
PDF
A novel stereoselective route to -lactams: diastereoselective synthesis of a key intermediate for carbapenem antibiotic (+)-PS-5
Okiko Miyata Yoko Fujiwara Ichiya Ninomiya and Takeaki Naito
pg 2861; DOI:
10.1039/P19930002861
PDF
1,5-Asymmetric induction in Lewis acid-promoted reactions of (5-alkoxy-2,4-dimethylpent-2-enyl)tributylstannanes and aldehydes
Aphiwat Teerawutgulrag and Eric J. Thomas
pg 2863; DOI:
10.1039/P19930002863
PDF
A short route to cephalostatin analogues
Andreas Kramer Ulrike Ullmann and Ekkehard Winterfeldt
pg 2865; DOI:
10.1039/P19930002865
PDF
Synthesis of benzo[g]chrysene 5,6-oxide and 7,8-oxide and their isomeric oxepines
Rajiv Agarwal and Derek R. Boyd
pg 2869; DOI:
10.1039/P19930002869
PDF
Biosynthesis of porphyrins and related macrocycles. Part 40. Synthesis of a spiro-lactam related to the proposed spiro-intermediate for porphyrin biosynthesis: inhibition of cosynthetase
W. Marshall Stark Craig J. Hawker Graham J. Hart Athena Philippides Paul M. Petersen J. David Lewis Finian J. Leeper and Alan R. Battersby
pg 2875; DOI:
10.1039/P19930002875
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Biosynthesis of porphyrins and related macrocycles. Part 41. Fate of oxygen atoms as precorrin-2 carrying eight labelled carboxyl groups (13C18O2H) is enzymatically converted into cobyrinic acid
Ram A. Vishwakarma Sarala Balachandran Alex I. D. Alanine N. Patrick J. Stamford Fumiyuki Kiuchi Finian J. Leeper and Alan R. Battersby
pg 2893; DOI:
10.1039/P19930002893
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Enzymatic synthesis of chiral 1-phenyl-1,2- and 1,3-diols via chiral epoxy alcohols
Mitsuhiro Takeshita Masatomo Miura and Yukiko Unuma
pg 2901; DOI:
10.1039/P19930002901
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New routes to 4-substituted steroids: synthesis of 4-cyanoprogesterone, a potent inhibitor of the enzyme 5-reductase
Margret Haase-Held Maria Hatzis and John Mann
pg 2907; DOI:
10.1039/P19930002907
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The synthesis of -hydroxy allylic phosphine oxides by palladium(II)-catalysed allylic acetate transposition
Jonathan Clayden and Stuart Warren
pg 2913; DOI:
10.1039/P19930002913
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Stereochemical course of the decarboxylation of 2-amino-2-methylmalonic acid by serine hydroxymethyltransferase
Neil R. Thomas Verne Schirch and David Gani
pg 2925; DOI:
10.1039/P19930002925
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Decarboxylation of 2-aminomalonic acid by serine hydroxymethyltransferase is, in fact, a stereospecific process
Neil R. Thomas Janet E. Rose and David Gani
pg 2933; DOI:
10.1039/P19930002933
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A convenient general method for the synthesis of pyrrole-2,5-dicarbaldehydes
Silvano Cadamuro Iacopo Degani Rita Fochi Antonella Gatti and Laura Piscopo
pg 2939; DOI:
10.1039/P19930002939
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Parasite glycoconjugates. Part 1. The synthesis of some early and related intermediates in the biosynthetic pathway of glycosyl-phosphatidylinositol membrane anchors
Sylvain Cottaz John S. Brimacombe and Michael A. J. Ferguson
pg 2945; DOI:
10.1039/P19930002945
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Studies on macrocyclic diterpenoids. Part 10. First total synthesis of ()-isosarcophytol-A
Yulin Li Weidong Li and Ying Li
pg 2953; DOI:
10.1039/P19930002953
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Vinyl cations in organic synthesis. Part 2. A novel synthesis of methylene-1H-indenes (benzofulvenes) by cyclisation of phenyl-substituted but-1-en-3-ynes
Franco Marcuzzi Ugo Azzena and Giovanni Melloni
pg 2957; DOI:
10.1039/P19930002957
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Reactions of diene-conjugated 1,3-dipolar intermediates: a versatile and efficient route to dibenz[c,e]azepines via benzonitrile o-arylbenzyl ylides
Kevin E. Cullen and John T. Sharp
pg 2961; DOI:
10.1039/P19930002961
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Chiral chlorobismuthines stabilized by the intramolecular coordination of an N,N-dimethylamino group: X-ray structure analysis, asymmetric induction at the bismuth centre, and dynamic behaviour in solution
Hitomi Suzuki Toshihiro Murafuji Yoshihiro Matano and Nagao Azuma
pg 2969; DOI:
10.1039/P19930002969
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The solvolytic ring opening of a 4,5-epoxy-3,6-dione steroid: preparation of potential aromatase inhibitors
Mitsuteru Numazawa and Mii Tachibana
pg 2975; DOI:
10.1039/P19930002975
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Vinyl epoxides: reagents for radical-induced DNA cleavage
Anthony P. Breen and John A. Murphy
pg 2979; DOI:
10.1039/P19930002979
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Selective reactions using N-(tert-butoxycarbonyl)-2-(tert-butyldimethylsiloxy)pyrrole: concise asymmetric syntheses of (+)-1-deoxy-8-epi-castanospermine and its enantiomer
Giovanni Casiraghi Fausta Ulgheri Pietro Spanu Gloria Rassu Luigi Pinna Giovanna Gasparri Fava Marisa Belicchi Ferrari and Giorgio Pelosi
pg 2991; DOI:
10.1039/P19930002991
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Novel efficient synthesis of 1-ethoxyvinyl esters using ruthenium catalysts and their use in acylation of amines and alcohols: synthesis of hydrophilic 3-N-acylated oxaunomycin derivatives
Yasuyuki Kita Hiroshi Maeda Kana Omori Takayuki Okuno and Yasumitsu Tamura
pg 2999; DOI:
10.1039/P19930002999
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Photoinduced molecular transformations. Part 144. One-carbon intercalation of - and -lactones involving the -scission of alkoxyl radicals as the key step: synthesis of - and ?-lactones with -substituents
Kazuhiro Kobayashi Hiroki Minakawa Hideo Sakurai Sachiko Kujime and Hiroshi Suginome
pg 3007; DOI:
10.1039/P19930003007
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Effects of cation binding to hydrophobic helical peptides on orientation, aggregation, and ion-channel activity in phospholipid bilayer membranes
Kazuya Otoda Shunsaku Kimura and Yukio Imanishi
pg 3011; DOI:
10.1039/P19930003011
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Chemo-enzymic synthesis of guanosine 5-diphosphomannose (GDP-mannose) and selected analogues
Jane E. Pallanca and Nicholas J. Turner
pg 3017; DOI:
10.1039/P19930003017
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Intramolecularly alkylated salen complexes: new models for coenzyme B12 with a cobalt-to-ligand carbon bridge
Bert van Arkel Juul L. van der Baan Sijbe Balt Friedrich Bickelhaupt Martinus W. G. de Bolster Irene E. Kingma Gerhard W. Klumpp Jan W. E. Moos and Anthony L. Spek
pg 3023; DOI:
10.1039/P19930003023
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Chemistry of Hantzsch cyclization: stereochemistry of the 2-hydroxy-1,2,3,4-tetrahydropyridine intermediate of Hantzsch cyclization. X-Ray molecular structure of diastereoisomers of 5-(2-cyanoethyl) 3-methyl 2-dimethoxymethyl-2-hydroxy-6-methyl-4-(3-nitrophenyl)-1,2,3,4-tetrahydropyridine-3,5-dicarboxylates
Toshihisa Ogawa Keita Matsumoto Katsuo Hatayama Kunihiro Kitamura and Yasuyuki Kita
pg 3033; DOI:
10.1039/P19930003033
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Candida cylindracea lipase-catalysed hydrolysis of methyl aziridine-2-carboxylates and -2,3-dicarboxylates
Maria Bucciarelli Arrigo Forni Irene Moretti Fabio Prati and Giovanni Torre
pg 3041; DOI:
10.1039/P19930003041
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Conference diary

pg ixc; DOI:
10.1039/P19930000ixc
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Issue 24


Index pages

pg A001; DOI:
10.1039/P199300BA001
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Front cover

pg X093; DOI:
10.1039/P199300FX093
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Back cover

pg X095; DOI:
10.1039/P199300BX095
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Contents pages

pg P193; DOI:
10.1039/P199300FP193
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Back matter

pg P199; DOI:
10.1039/P199300BP199
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Anomalous reactivity of sodium phenyl selenide
Polly A. Harrison Lorraine Murtagh and Christine L. Willis
pg 3047; DOI:
10.1039/P19930003047
PDF
Reactions of methylated 5-chloro-1,2,3-thiadiazolium salts with cyclohexane-1,3-diones: X-ray crystal structure analysis of the thiapentalenic products
Gerrit L'abbé Lieve Bastin Dominique Vlieghe and Luc Van Meervelt
pg 3051; DOI:
10.1039/P19930003051
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Use of functionalised ynamines in a hetero-Diels–Alder approach to dihydronaphtho[1,2-b]pyrans and indeno[1,2-b]pyrans
Jason Bloxham and Colin P. Dell
pg 3055; DOI:
10.1039/P19930003055
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Facile aromatisation of abscisic acid
Michael H. Beale Anqi Chen Polly A. Harrison and Christine L. Willis
pg 3061; DOI:
10.1039/P19930003061
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Oxidation of octadecatrienoic acids in the red alga Lithothamnion corallioides: structural and stereochemical studies of conjugated tetraene fatty acids and bis allylic hydroxy acids
Mats Hamberg
pg 3065; DOI:
10.1039/P19930003065
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Synthesis of analogues of squalene as potential anti-fungal agents
Albert Duriati Michel Jung John Mann and Garrick P. Smith
pg 3073; DOI:
10.1039/P19930003073
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Organic heterocyclothiazenes. Part 18. 1,3,2-Dithiazolium salts and 1,3,2-dithiazolethiones
Michael A. Gray and Charles W. Rees
pg 3077; DOI:
10.1039/P19930003077
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Formal syntheses of hepoxilin B3, trioxilin B3 and substances effective against rice blast disease and total syntheses of 11(R), 12(S), 13(S)-trihydroxyoctadeca-9(Z), 15(Z)-dienoic acid
Wen-Lian Wu and Yu-Lin Wu
pg 3081; DOI:
10.1039/P19930003081
PDF
Synthesis and properties of N-tritylthio nucleoside derivatives and reductive removal of the tritylthio group by use of tributyltin hydride and tris(trimethylsilyl)silane
Mitsuo Sekine and Kohji Seio
pg 3087; DOI:
10.1039/P19930003087
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Anodic cyanation of tert-butylated anisoles: competitive aromatic additions and substitutions
Kunihisa Yoshida Kazusada Takeda and Takayuki Fueno
pg 3095; DOI:
10.1039/P19930003095
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Application of homochiral lithium amide base chemistry to a thiane oxide system
Richard Armer Michael J. Begley Paul J. Cox Andrew Persad and Nigel S. Simpkins
pg 3099; DOI:
10.1039/P19930003099
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Stereoselective synthesis using a thiane oxide system as a disposable template
Richard Armer Michael J. Begley Paul J. Cox Andrew Persad and Nigel S. Simpkins
pg 3105; DOI:
10.1039/P19930003105
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The effect of added salts on enantioselective transformations of cyclic ketones by chiral lithium amide bases
Barry J. Bunn Nigel S. Simpkins Zoé Spavold and Michael J. Crimmin
pg 3113; DOI:
10.1039/P19930003113
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Anodic oxidation of 3,5-dihalogenotyrosines as a model reaction for the biogenesis of the cavernicolins, metabolites of the verongid sponge Aplysina cavernicola
Marino Cavazza Graziano Guella Lamberto Nucci Francesco Pergola Nicola Bicchierini and Francesco Pietra
pg 3117; DOI:
10.1039/P19930003117
PDF
Hemifistularin 3: a degraded peptide or biogenetic precursor? Isolation from a sponge of the order verongida from the coral sea or generation from base treatment of 11-oxofistularin 3
Ines Mancini Graziano Guella Pierre Laboute Cécile Debitus and Francesco Pietra
pg 3121; DOI:
10.1039/P19930003121
PDF
Medium-sized cyclophanes. Part 31. Synthesis and electrophilic substitution of 8-substituted [2]metacyclo[2](1,3)pyrenophanes
Takehiko Yamato Akira Miyazawa and Masashi Tashiro
pg 3127; DOI:
10.1039/P19930003127
PDF
Direct esterification of phosphates with various halides and its application to synthesis of cAMP alkyl triesters
Toshiaki Furuta Hiromi Torigai Tomoko Osawa and Michiko Iwamura
pg 3139; DOI:
10.1039/P19930003139
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General method for the synthesis of enantiomerically pure -hydroxy--amino acids, containing fluorine atoms in the side chains. Case of stereochemical distinction between methyl and trifluoromethyl groups. X-Ray crystal and molecular structure of the nickel(II) complex of (2S,3S)-2(trifluoromethyl)threonine
Vadim A. Soloshonok Valeri P. Kukhar Sergei V. Galushko Nataly Yu. Svistunova Dimitri V. Avilov Nadia A. Kuz'mina Nicolai I. Raevski Yuri T. Struchkov Alexander P. Pysarevsky and Yuri N. Belokon
pg 3143; DOI:
10.1039/P19930003143
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Trimethylsilyl trifluoromethanesulfonate-promoted cycloaddition of nitrones with silyl enol ethers: synthesis and reactivity of 5-siloxyisoxazohdines
Chiara Camiletti Dilip D. Dhavale Luca Gentiluccia and Claudio Trombini
pg 3157; DOI:
10.1039/P19930003157
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New decarboxylation, de-ethoxycarbonylation and desulfonylation, followed by sulfenylation of some half-esters of malonic acids and -sulfonylmalonic esters
Blanka Wladislaw Liliana Marzorati and Claudio L. Donnici
pg 3167; DOI:
10.1039/P19930003167
PDF
Regioselective free radical cyclization: a general method for the synthesis of the spiro[4.4]nonane system of fredericamycin A
A. V. Rama Rao Ashok K. Singh Komandla Malla Reddy and Krishnan Ravikumar
pg 3171; DOI:
10.1039/P19930003171
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Corrigenda
Gunther Bentz Jürgen Werry Helmut Stamm Makoto Watanabe Mineo Komota Masamichi Nishimura Shuki Araki and Yasuo Butsugan
pg 3177; DOI:
10.1039/P19930003177
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Conference diary

pg viis; DOI:
10.1039/P1993000viis
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